Double-sided laser heating system for in situ high pressure-high temperature monochromatic X-ray diffraction at the ESRF

被引:72
作者
Schultz, E
Mezouar, M
Crichton, W
Bauchau, S
Blattmann, G
Andrault, D
Fiquet, G
Boehler, R
Rambert, N
Sitaud, B
Loubeyre, P
机构
[1] ESRF, F-38000 Grenoble, France
[2] Univ Paris 06, IMPMC, F-75015 Paris, France
[3] CEA, Valduc, F-21120 Is Sur Tille, France
[4] CEA, DPTA, F-91680 Bruyeres Le Chatel, France
关键词
laser heating; diamond anvil cell; high pressure; high temperature; monochromatic XRD; spectral radiometry;
D O I
10.1080/08957950500076031
中图分类号
O4 [物理学];
学科分类号
0702 ;
摘要
A new double-sided laser heating system optimized for monochromatic X-ray diffraction at high pressure and high temperature has been developed at beamline ID27 of the European Synchrotron Radiation Facility (ESRF). The main components of this system including optimized focusing optics to produce a large and homogenous heated area, optimized mirror optics for temperature measurements and a state-of-the-art diffraction setup are described in details. Preliminary data collected at high pressure and high temperature on tungsten and iron are presented.
引用
收藏
页码:71 / 83
页数:13
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