Determination of aldicarb, propoxur, carbofuran, carbaryl and methiocarb residues in honey by HPLC with post-column derivatization and fluorescence detection after elution from a florisil column

被引：0
|
作者：
Koc, Feride [1 ]
Yigit, Yusuf [2 ]
Das, Yavuz Kursad [3 ]
Gurel, Yasemin [2 ]
Yaral, Cevdet [4 ]
机构：
[1] Ataturk Univ, Fac Vet Med, Dept Pharmacol & Toxicol, TR-25400 Erzurum, Turkey
[2] Cent Vet Control & Res Inst, Toxicol Lab, Ankara, Turkey
[3] 19 Mayis Univ, Fac Vet Med, Dept Pharmacol & Toxicol, Samsun, Turkey
[4] Cent Vet Control & Res Inst, Genet Lab, Ankara, Turkey
来源：
JOURNAL OF FOOD AND DRUG ANALYSIS | 2008年 / 16卷 / 03期
关键词：
honey; liquid chromatography; post-column derivatization; N-methylcarbamate pesticide; residue; florisil;
D O I：
暂无
中图分类号：
TS2 [食品工业];
学科分类号：
0832 ;
摘要：
The aim of this study was to develop an easy analytical method for determining aldicarb, propoxur, carbofuran, carbaryl and methiocarb residues in honey by high performance liquid chromatography with post-column derivatization and fluorescence detection (HPLC/PCD-FL) for routine analysis. A florisil packed column was used in sample preparation step and showed good performance. The recoveries ranged between 72.02 and 92.02% for various spiking levels (50, 100, 200 ng/g). The limits of detection were 4-5 ng/g, depending on different N-methylcarbamate pesticides. The extraction method used in the present study was easy, inexpensive, and rapid. Thus, it could be used efficiently in the routine monitoring studies.
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页码：39 / 45
页数：7
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