Study on the thermal and mechanical properties of epoxy-nanoclay composites: The effect of ultrasonic stirring time

被引:52
作者
Wang, Jinwei [1 ]
Qin, Shuchao [1 ]
机构
[1] Univ Sci & Technol Beijing, Sch Mat Sci & Engn, Dept Mat Phys & Chem, Beijing Key Lab Corros Eros & Surface Technol, Beijing 100083, Peoples R China
关键词
nanocomposite; thermal properties; mechanical properties; epoxy; ultrasonic stirring;
D O I
10.1016/j.matlet.2007.01.058
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Epoxy-clay nanocomposites were synthesized with organophilic montmorillonite and diglycidyl ether of bisphenol A by using the in-situ polymerization under ultrasonic treatment. The clay layers were found to be separated further with the increase in the duration of ultrasonic stirring as measured from the X-ray diffraction measurements. Thermogravimetric analysis provided the fact that the maximum thermal decomposition temperatures increased with the increase in the duration of ultrasonic stirring. However, both the glass transition temperature and the storage moduli of the composites decreased with the increase of ultrasonic stirring time as measured from the dynamic mechanical analysis. (c) 2007 Elsevier B.V All rights reserved.
引用
收藏
页码:4222 / 4224
页数:3
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