Combining high time and angular resolutions: time-resolved X-ray powder diffraction using a multi-channel analyser detector

被引:11
作者
Choe, Hyeokmin [1 ]
Gorfman, Semen [1 ]
Hinterstein, Manuel [2 ,3 ]
Ziolkowski, Michael [1 ]
Knapp, Michael [2 ]
Heidbrink, Stefan [1 ]
Vogt, Marco [1 ]
Bednarcik, Jozef [4 ]
Berghaeuser, Andreas [5 ]
Ehrenberg, Helmut [3 ]
Pietsch, Ullrich [1 ]
机构
[1] Univ Siegen, Dept Phys, D-57068 Siegen, Germany
[2] Univ New S Wales, Sch Mat Sci & Engn, Sydney, NSW 2052, Australia
[3] Karlsruhe Inst Technol, Inst Appl Mat, D-76021 Karlsruhe, Germany
[4] Deutsches Elektronen Synchrotron DESY, D-22603 Hamburg, Germany
[5] Univ Hamburg, D-20146 Hamburg, Germany
关键词
data acquisition systems; time-resolved X-ray powder diffraction; multi-channel analyser detectors; FERROELECTRIC POLARIZATION DATA; EXTERNAL ELECTRIC-FIELD; CRYSTALLOGRAPHY; CERAMICS; CRYSTALS; SCIENCE;
D O I
10.1107/S1600576715004598
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
The design and testing of the new MAD-STROBO data acquisition system are reported. The system realizes stroboscopic collection of high-resolution X-ray powder diffraction profiles under a dynamically applied electric field. It synchronizes an externally applied stimulus and detected X-ray photons. The feasibility of detecting sub-millidegree shifts of powder diffraction profiles with microsecond time resolution is demonstrated. MAD-STROBO may be applied for the investigation of various macroscopic and domain-related processes induced by an external perturbation, such as elasticity or piezoelectricity.
引用
收藏
页码:970 / 974
页数:5
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