Belok/XSA Diffraction Beamline for Studying Crystalline Samples at Kurchatov Synchrotron Radiation Source

被引:196
作者
Svetogorov, Roman D. [1 ]
Dorovatovskii, Pavel, V [1 ]
Lazarenko, Vladimir A. [1 ]
机构
[1] Natl Res Ctr, Kurchatov Inst, 1 Akad Kurchatova Pl, Moscow 123182, Russia
关键词
crystal structures; diffraction beamline; Kurchatov synchrotron radiation source; powder diffraction; single-crystal diffraction; STATION;
D O I
10.1002/crat.201900184
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
Introduction of "Belok/XSA" beamline-modernization is presented here with commissioning of a modern synchrotron beamline with unique capabilities for the structural analysis of single and polycrystalline samples. The beamline is designed to perform important tasks in modern crystallography, such as solving and refining the atomic structure using the single- and polycrystal method, studying the real (defective) structure, and analyzing the distribution of electron density in crystals, it is also possible to study rapidly occurring processes, for example, temperature phase transitions. Due to the speed of data accumulation and a registration over a large solid angle, the method allows to study large numbers of samples. This beamline has become extremely demanded in the chemical, biological, material science, and archaeological community in Russia.
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页数:6
相关论文
共 12 条
  • [1] iMOSFLM: a new graphical interface for diffraction-image processing with MOSFLM
    Battye, T. Geoff G.
    Kontogiannis, Luke
    Johnson, Owen
    Powell, Harold R.
    Leslie, Andrew G. W.
    [J]. ACTA CRYSTALLOGRAPHICA SECTION D-BIOLOGICAL CRYSTALLOGRAPHY, 2011, 67 : 271 - 281
  • [2] OLEX2: a complete structure solution, refinement and analysis program
    Dolomanov, Oleg V.
    Bourhis, Luc J.
    Gildea, Richard J.
    Howard, Judith A. K.
    Puschmann, Horst
    [J]. JOURNAL OF APPLIED CRYSTALLOGRAPHY, 2009, 42 : 339 - 341
  • [3] Scaling and assessment of data quality
    Evans, P
    [J]. ACTA CRYSTALLOGRAPHICA SECTION D-STRUCTURAL BIOLOGY, 2006, 62 : 72 - 82
  • [4] XDS
    Kabsch, Wolfgang
    [J]. ACTA CRYSTALLOGRAPHICA SECTION D-BIOLOGICAL CRYSTALLOGRAPHY, 2010, 66 : 125 - 132
  • [5] The Belok station for protein crystallography on the synchrotron radiation beam from the bending magnet in the Sibir-2 storage ring
    Kheiker, D. M.
    Kovalchuk, M. V.
    Shilin, Yu. N.
    Shishkov, V. A.
    Sulyanov, S. N.
    Dorovatovskii, P. V.
    Rusakov, A. A.
    [J]. CRYSTALLOGRAPHY REPORTS, 2007, 52 (02) : 358 - 364
  • [6] SHADOW - A SYNCHROTRON RADIATION RAY TRACING PROGRAM
    LAI, B
    CERRINA, F
    [J]. NUCLEAR INSTRUMENTS & METHODS IN PHYSICS RESEARCH SECTION A-ACCELERATORS SPECTROMETERS DETECTORS AND ASSOCIATED EQUIPMENT, 1986, 246 (1-3) : 337 - 341
  • [7] High-Throughput Small-Molecule Crystallography at the "Belok' Beamline of the Kurchatov Synchrotron Radiation Source: Transition Metal Complexes with Azomethine Ligands as a Case Study
    Lazarenko, Vladimir A.
    Dorovatovskii, Pavel V.
    Zubavichus, Yan V.
    Burlov, Anatolii S.
    Koshchienko, Yurii V.
    Vlasenko, Valery G.
    Khrustalev, Victor N.
    [J]. CRYSTALS, 2017, 7 (11):
  • [8] Efficiency of the focusing channel of the Belok Station in the Sibir-2 storage ring
    Molodenskii, D. S.
    Dorovatovskii, P. V.
    Zabrodskii, V. V.
    Kheiker, D. M.
    [J]. CRYSTALLOGRAPHY REPORTS, 2010, 55 (05) : 896 - 900
  • [9] Press WH., 1990, COMPUT PHYS, V4, P669, DOI [10.1063/1.4822961, DOI 10.1063/1.4822961]
  • [10] New Python']Python-based methods for data processing
    Sauter, Nicholas K.
    Hattne, Johan
    Grosse-Kunstleve, Ralf W.
    Echols, Nathaniel
    [J]. ACTA CRYSTALLOGRAPHICA SECTION D-STRUCTURAL BIOLOGY, 2013, 69 : 1274 - 1282