The firing procedure influences properties of a zirconia core ceramic

被引:42
作者
Oilo, Marit [1 ]
Gjerdet, Nils Roar [1 ]
Tvinnereim, Helene M. [1 ]
机构
[1] Univ Bergen, Dept Oral Sci, N-5009 Bergen, Norway
关键词
dental ceramics; zirconia; heat treatment; flexural strength; microhardness; fractography;
D O I
10.1016/j.dental.2007.04.008
中图分类号
R78 [口腔科学];
学科分类号
1003 ;
摘要
Objectives. High-strength ceramics for dental restoration are used as an understructure (core) that subsequently is covered by veneering ceramic. The veneering process involves a firing procedure at high temperatures at least once, usually two to five times. The aim of this study was to investigate whether these firing procedures affect the mechanical properties of a zirconia ceramic. Methods. Thirty-three specimens of an industrially sintered yttria -stabilized zirconia ceramic (DC Zircon, DCS Dental AG, Allschwil, Switzerland) were cut into bars (1.2 mm x 4 mm x 20 mm). one set of specimens (n = 13) remained untreated (controls). Another set of specimens (n = 10) was heat-treated once, corresponding to the first step of the veneering process. The third set of specimens (n = 10) was heat-treated five times to mimic the full veneering process. Flexural strength, microhardness, dimensions and surface roughness were measured. The fracture patterns were assessed by light microscopy. Results. The untreated specimens showed a statistically significant higher flexural strength (20%) and microhardness (9%) than both of the test groups (p <= 0.001). No significant differences were found for fracture patterns, dimensions or surface roughness. Significance. The heat treatment associated with the veneering procedure on a zirconia core material reduced the flexural strength of the core after the first firing. Subsequent firings were not detrimental to the properties measured. (C) 2007 Academy of Dental Materials. Published by Elsevier Ltd. All rights reserved.
引用
收藏
页码:471 / 475
页数:5
相关论文
共 34 条
[1]   Fatigue and static crack propagation in yttria-stabilized tetragonal zirconia polycrystals: Crack growth micromechanisms and precracking effects [J].
Alcala, J ;
Anglada, M .
JOURNAL OF THE AMERICAN CERAMIC SOCIETY, 1997, 80 (11) :2759-2772
[2]   Instrumented micro-indentation of zirconia ceramics [J].
Alcalá, J .
JOURNAL OF THE AMERICAN CERAMIC SOCIETY, 2000, 83 (08) :1977-1984
[3]  
[Anonymous], 1995, 6872 ISO
[4]   GRAIN-BOUNDARY RESISTIVITY IN ZIRCONIA-BASED MATERIALS - EFFECT OF SINTERING TEMPERATURES AND IMPURITIES [J].
BADWAL, SPS .
SOLID STATE IONICS, 1995, 76 (1-2) :67-80
[5]   Influence of firing cycles on the margin distortion of 3 all-ceramic crown systems [J].
Balkaya, MC ;
Cinar, A ;
Pamuk, S .
JOURNAL OF PROSTHETIC DENTISTRY, 2005, 93 (04) :346-355
[6]   The effect of veneering and heat treatment on the flexural strength of Empress® 2 ceramics [J].
Cattell, MJ ;
Palumbo, RP ;
Knowles, JC ;
Clarke, RL ;
Samarawickrama, DYD .
JOURNAL OF DENTISTRY, 2002, 30 (04) :161-169
[7]   What future for zirconia as a biomaterial? [J].
Chevalier, J .
BIOMATERIALS, 2006, 27 (04) :535-543
[8]   The influence of surface modification techniques on the performance of a Y-TZP dental ceramic [J].
Curtis, AR ;
Wright, AJ ;
Fleming, GJP .
JOURNAL OF DENTISTRY, 2006, 34 (03) :195-206
[9]   Characterization of damage modes in dental ceramic bilayer structures [J].
Deng, Y ;
Lawn, BR ;
Lloyd, IK .
JOURNAL OF BIOMEDICAL MATERIALS RESEARCH, 2002, 63 (02) :137-145
[10]   Influence of surface finish and residual stresses on the ageing sensitivity of biomedical grade zirconia [J].
Deville, S ;
Chevalier, J ;
Gremillard, L .
BIOMATERIALS, 2006, 27 (10) :2186-2192