Sensitivity enhancement in solid-state 13C NMR of synthetic polymers and biopolymers by 1H NMR detection with high-speed magic angle spinning

被引：148
作者：
Ishii, Y
Yesinowski, JP
Tycko, R
机构：
[1] NIDDKD, Chem Phys Lab, NIH, Bethesda, MD 20892 USA
[2] USN, Res Lab, Div Chem, Washington, DC 20375 USA
来源：
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY | 2001年 / 123卷 / 12期
关键词：
D O I：
10.1021/ja015505j
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
引用
收藏
页码：2921 / 2922
页数：2
相关论文
共 21 条
[1]   Amyloid fibril formation by Aβ16-22, a seven-residue fragment of the Alzheimer's β-amyloid peptide, and structural characterization by solid state NMR [J].
Balbach, JJ ;
Ishii, Y ;
Antzutkin, ON ;
Leapman, RD ;
Rizzo, NW ;
Dyda, F ;
Reed, J ;
Tycko, R .
BIOCHEMISTRY, 2000, 39 (45) :13748-13759
[2]   CORRELATION OF PROTON AND N-15 CHEMICAL-SHIFTS BY MULTIPLE QUANTUM NMR [J].
BAX, A ;
GRIFFEY, RH ;
HAWKINS, BL .
JOURNAL OF MAGNETIC RESONANCE, 1983, 55 (02) :301-315
[3]   NUCLEAR MAGNETIC RESONANCE IN THE CESIUM HALIDES [J].
BLOEMBERGEN, N ;
SOROKIN, PP .
PHYSICAL REVIEW, 1958, 110 (04) :865-875
[4]   HETERONUCLEAR CORRELATION SPECTROSCOPY IN ROTATING SOLIDS [J].
CARAVATTI, P ;
BRAUNSCHWEILER, L ;
ERNST, RR .
CHEMICAL PHYSICS LETTERS, 1983, 100 (04) :305-310
[5]  
Ernst R. R., 1987, PRINCIPLES NUCL MAGN, P148
[6]  
ERNST RR, 1987, PRINCIPLES NUCL MAGN, P349
[7]   Solid-state nuclear magnetic resonance spectra of dipolar-coupled multi-spin systems under fast magic angle spinning [J].
Filip, C ;
Hafner, S ;
Schnell, I ;
Demco, DE ;
Spiess, HW .
JOURNAL OF CHEMICAL PHYSICS, 1999, 110 (01) :423-440
[8]   NUCLEAR DOUBLE RESONANCE IN ROTATING FRAME [J].
HARTMANN, SR ;
HAHN, EL .
PHYSICAL REVIEW, 1962, 128 (05) :2042-&
[9]   Sensitivity enhancement in solid state 15N NMR by indirect detection with high-speed magic angle spinning [J].
Ishii, Y ;
Tycko, R .
JOURNAL OF MAGNETIC RESONANCE, 2000, 142 (01) :199-204
[10]   IMPROVED RESOLUTION OF SMALL RESONANCE SHIFTS OF DILUTE NUCLEAR SPIN SYSTEMS IN SOLIDS BY PULSED DOUBLE RESONANCE [J].
MANSFIELD, P ;
GRANNELL, PK .
JOURNAL OF PHYSICS PART C SOLID STATE PHYSICS, 1971, 4 (10) :L197-+
123