Preparation of Au2S3 and nanocrystalline gold by sonochemical method

被引：14

作者：

Kristl, M ^{[1
]}

Drofenik, M ^{[1
]}

机构：

[1] Univ Maribor, Fac Chem & Chem Engn, SI-2000 Maribor, Slovenia

来源：

INORGANIC CHEMISTRY COMMUNICATIONS | 2003年 / 6卷 / 12期

关键词：

sonochemical reaction; sulfides; nanostructures;

D O I：

10.1016/j.inoche.2003.08.027

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

We report a new synthesis of Au2S3 by a sonochemical reaction between Au(CH3COO)(3) and S in decalin at room temperature in nitrogen atmosphere. When gold acetate is sonicated under similar conditions without the presence of sulfur, nanocrystalline gold is formed. The products were characterized by X-ray powder diffraction, transmission electron microscope and thermal analysis (TG and DSC). The synthesis procedure is substantially simpler than the previously reported methods. (C) 2003 Elsevier B.V. All rights reserved.

引用

页码：1419 / 1422

页数：4

共 24 条

[1]

ANTONY U, 1890, GAZZ CHIM ITAL, V20, P61

[2] LOW TEMPERATURE SUPPRESSION BY CHLORINE OF DIFFUSION OF GOLD IN SILVER CHLORIDE [J].

BATRA, AP ;

LASKAR, AL ;

SLIFKIN, L .

JOURNAL OF PHYSICS AND CHEMISTRY OF SOLIDS, 1969, 30 (08) :2053-&

[3] STRUCTURAL-PROPERTIES OF AMORPHOUS BULK FE, CO AND FE-CO BINARY-ALLOYS [J].

BELLISSENT, R ;

GALLI, G ;

HYEON, T ;

MAGAZU, S ;

MAJOLINO, D ;

MIGLIARDO, P ;

SUSLICK, KS .

PHYSICA SCRIPTA, 1995, T57 :79-83

[4] MAGNETIC-PROPERTIES OF AMORPHOUS IRON [J].

GRINSTAFF, MW ;

SALAMON, MB ;

SUSLICK, KS .

PHYSICAL REVIEW B, 1993, 48 (01) :269-273

[5]

GUBTIER A, 1922, ANORG ALLG CHEM, V121, P266

[6]

HIRSCH H, 1966, CR ACAD SCI B PHYS, V263, P1328

[7] Grain size measurement of nanocrystalline gold by X-ray diffraction method [J].

Inami, T ;

Kobiyama, M ;

Okuda, S ;

Maeta, H ;

Ohtsuka, H .

NANOSTRUCTURED MATERIALS, 1999, 12 (5-8) :657-660

[8]

JOHNSON BF, 1973, COMPREHENSIVE INORGA, pCH29

[9] Synthesis of nanocrystalline MoSe2 by sonochemical reaction of Se with Mo(CO)6 [J].

Kristl, M ;

Drofenik, M .

INORGANIC CHEMISTRY COMMUNICATIONS, 2003, 6 (01) :68-70

[10] Sonochemical synthesis of nanocrystalline silver tellurides Ag2Te and Ag7Te4 [J].

Li, B ;

Xie, Y ;

Liu, Y ;

Huang, JX ;

Qian, YT .

JOURNAL OF SOLID STATE CHEMISTRY, 2001, 158 (02) :260-263

← 1 2 3 →