5-[(8-Hydroxyquinolin-2-ylamino)-methylene]-2,2-dimethyl-1,3-dioxane-4,6-dione

被引:0
作者
da Silva, Luiz Everson
de Sousa, Paulo Teixeira, Jr.
Dall'Oglio, Evandro Luiz
Foro, Sabine
机构
[1] Tech Univ Darmstadt, Clemens Schopf Inst Organ Chem & Biochem, D-64287 Darmstadt, Germany
[2] Univ Fed Mato Grosso, Dept Quim, BR-78060900 Cuiaba, MT, Brazil
关键词
D O I
10.1107/S160053680703214X
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
\In the title compound, C16H14N2O5, the 1,3-dioxane-4,6-dione ring is in an envelope conformation. The C-N-C-C torsion angle between the nearly planar quinoline ring system carrying the OH group and the 1,3-dioxane-4,6-dione unit is -177.1 (1)degrees. The NH group has an intramolecular contact to a carbonyl O atom, forming a six-membered ring, and also an intermolecular contact to the carbonyl 0 atom. One intramolecular O-H center dot center dot center dot N and two intermolecular C-H center dot center dot center dot O hydrogen bonds are also observed. Two molecules are connected by these hydrogen bonds, forming layers.
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收藏
页码:O3439 / U2825
页数:10
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