(E)-N′-(5-Bromo-2-hydroxy-3-methoxybenzylidene)-1H-indole-3-carbohydrazide

被引:0
|
作者
Li, Xiao-Yan [1 ]
机构
[1] Zibo Vocat Inst, Zibo 255314, Peoples R China
来源
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2011年 / 67卷
关键词
data-to-parameter ratio = 12.1; mean σ(C-C) = 0.009 Å; R factor = 0.051; single-crystal X-ray study; T = 298 K; wR factor = 0.125;
D O I
10.1107/S1600536811039195
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
There are three independent moleculesi n the asymmetric unit of the title compound, C18H16BrN3O3, in which the dihedral angles between the indole and benzene rings are 76.9 (2), 4.9 (2), and 70.9 (2)degrees. All three molecules exist in a trans configuration with respect to the methylidene units. In each molecule, there is one intramolecular O-H center dot center dot center dot N hydrogen bond. In the crystal, N-H center dot center dot center dot O hydrogen bonds occur.
引用
收藏
页码:O2815 / +
页数:13
相关论文
共 50 条
  • [31] 2-Methyl-1-phenylsulfonyl-1H-indole-3-carbaldehyde
    Ramathilagam, C.
    Saravanan, V.
    Mohanakrishnan, A. K.
    Umarani, P. R.
    Manivannan, V.
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O2614 - +
  • [32] 5-Bromo-3-(3-fluorophenylsulfinyl)-2-methyl-1-benzofuran
    Choi, Hong Dae
    Seo, Pil Ja
    Lee, Uk
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : 02491 - +
  • [33] rac-(Z)-Methyl 1-benzyl-3-[(3-hydroxy-quinuclidin-2-ylidene)methyl]-1H-indole-6-carboxylate
    Penthala, Narsimha Reddy
    Ponugoti, Purushotham Rao
    Parkin, Sean
    Crooks, Peter A.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : O3111 - +
  • [34] (E)-2-Bromo-1-[2-(2-nitrostyryl)-1-phenylsulfonyl-1H-indol-3-yl]ethanone
    Kanchanadevi, J.
    Anbalagan, G.
    Saravanan, V.
    Mohanakrishnan, A. K.
    Gunasekaran, B.
    Manivannan, V.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2014, 70 : 0149 - +
  • [35] 2-{[2-(2-Hydroxy-3-methoxybenzylidene)hydrazin-1-ylidene]methyl}-6-methoxyphenol
    Lu, Rong
    Wang, Wenxia
    Lu, Xingqiang
    Zhao, Shunsheng
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O2702 - +
  • [36] {2-[(2-Bromo-5-methoxybenzylidene)amino]-4,5,6,7-tetrahydrobenzo[b] thiophen-3-yl}(phenyl) methanone
    Kaur, Manpreet
    Jasinski, Jerry P.
    Yamuna, Thammarse S.
    Yathirajan, H. S.
    Byrappa, K.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2014, 70 : O581 - +
  • [37] 1-(5-Bromo-2-oxoindolin-3-ylidene)thiosemicarbazone
    Bandeira, Katlen C. T.
    Bresolin, Leandro
    Nather, Christian
    Jess, Inke
    Oliveira, Adriano B.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2013, 69 : O1251 - +
  • [38] (E)-4-Bromo-N-{(E)-3-[(4-bromo-2-methylphenyl)imino]butan-2-ylidene}-2-methylaniline
    Yao, Jin-Li
    Zhang, Xu
    Li, Hong-Yan
    Ye, Jian-Qing
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2013, 69 : O199 - +
  • [39] 5-Bromo-2-methyl-3-(3-methylphenyl-sulfinyl)-1-benzofuran
    Choi, Hong Dae
    Seo, Pil Ja
    Lee, Uk
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2014, 70 : O320 - +
  • [40] 4-Hydroxy-3-[(E)-3-phenylprop-2-enoyl]-2H-chromen-2-one
    Ghouili, Afef
    Ben Hassen, Rached
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O2209 - U2106