Synthesis, crystal structure and magnetic property of an iron(III) coordination polymer with N-acyl-salicylhydrazide ligand

被引：3
|
作者：
Qin, Suni [1 ,2 ]
Zu, Chao [1 ]
Chen, Zilu [1 ]
Huang, Wanyun [1 ,2 ]
Qin, Jiangke [1 ]
Liang, Fupei [1 ]
机构：
[1] Guangxi Normal Univ, Key Lab Chem & Mol Engn Med Resources, Minist Educ China, Sch Chem & Chem Engn, Guilin 541004, Peoples R China
[2] Nanjing Univ, State Key Lab Coordinat Chem, Inst Coordinat Chem, Sch Chem & Chem Engn, Nanjing 210093, Peoples R China
来源：
INORGANIC CHEMISTRY COMMUNICATIONS | 2011年 / 14卷 / 06期
基金：
中国国家自然科学基金;
关键词：
Coordination polymer; Iron(III); N-acyl-salicylhydrazide; Crystal structure; Magnetic property; 24-MEMBERED OCTANUCLEAR; 18-MEMBERED HEXANUCLEAR; BRIDGING LIGAND; STERIC CONTROL; METALLAMACROCYCLE; 18-METALLACROWN-6; BIOACTIVITY; NUCLEARITY; HEXADECANUCLEAR;
D O I：
10.1016/j.inoche.2011.03.066
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
A one-dimensional coordination polymer of iron(III) with N-dehydroabietoyl-salicylhydrazide (H3L) ligand, [Fe (HL)Cl(CH3OH)](n)center dot nCH(3)OH (1), was synthesized and characterized by single-crystal X-ray diffraction, elemental analysis, and infrared spectra analysis. The N-dehydroabietoyl-salicylhydrazide ligand in the compound is doubly deprotonated and acts as a tetradentate ligand to Fe(III) ions in tridentate-monodentate/back-to-back fashion, giving rise to a linear chain structure. The 1D chain is further extended to 2D supramolecular network by intermolecular hydrogen bonds. The magnetic study of the compound indicates an antiferromagnetic coupling interaction between Fe(III) ions. (C) 2011 Elsevier B.V. All rights reserved.
引用
收藏
页码：1036 / 1038
页数：3
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