Effect of Different Mineralizers in the Sonochemical Synthesis of Self-Assembled Nanorods Vanadium Oxide

被引:0
作者
Taufiq-Yap, Y. H. [1 ,2 ]
Hoh, J. R. Joshua [1 ,2 ]
Wong, Y. C. [1 ,2 ]
机构
[1] Univ Putra Malaysia, Ctr Excellence Catalysis Sci & Technol, Upm Serdang 43400, Selangor Darul, Malaysia
[2] Univ Putra Malaysia, Fac Sci, Dept Chem, Upm Serdang 43400, Selangor Darul, Malaysia
关键词
Sonochemical treatment; Mineralizer; Vanadium oxide; Nanorods; ULTRASOUND; CATALYSTS;
D O I
暂无
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
The effects of different potassium salts (KNO(3) and KCl) as mineralizer on the synthesis of self-assembled nanorods vanadium pentoxide, V(2)O(5) via sonochemical treatment were studied at different duration i.e., 30, 60, 90 and 120 min. All the materials synthesized were further characterized by x-ray diffraction, scanning electron microscopy and transmission electron microscopy. X-ray diffraction patterns revealed that the potassium ion from the mineralizers reacted with the V(2)O(5) after prolonged sonochemical treatment duration. The morphology of the V(2)O(5) changed from platelet-like structures into nanorods after 90 min of sonochemical treatment. TEM micrographs show the process of formation of the self-assembled V(2)O(5) nanorod bundles with increased sonochemical treatment duration.
引用
收藏
页码:505 / 510
页数:6
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