Diethyl 4,5-diphenyl-3,6-bis(trimethylsilyl)benzene-1,2-dicarboxylate

被引：3
|
作者：
Zhang, Jing [1 ]
Qu, Hongmei [1 ]
Zhang, Zhenyu [1 ]
Zhou, Lishan [2 ]
机构：
[1] Tianjin Univ, Sch Chem Engn & Technol, Tianjin 300072, Peoples R China
[2] Tianjin Res & Design Inst Chem Ind, Tianjin 300131, Peoples R China
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2011年 / 67卷
关键词：
POLYMERIZATION VON ACETYLEN;
D O I：
10.1107/S160053681102397X
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
In the title compound, C30H38O4Si2, the two phenyl rings are twisted away from the central benzene ring by 70.28 (8) and 67.42 (7)degrees. The two Si atoms attached to the benzene ring deviate in opposite directions from the ring plane by 0.258 (3) and 0.206 (3) angstrom, respectively. One ethyl group is disordered over two conformations in a 0.568 (5):0.432 (5) ratio. The crystal packing exhibits weak intermolecular C-H center dot center dot center dot O interactions.
引用
收藏
页码：O1864 / U2224
页数：13
相关论文
共 50 条
  • [1] Tetramethyl 4,4′-carbonylbis(benzene-1,2-dicarboxylate)
    Zhu, Xin-Yi
    Gao, Guo-Wei
    Men, Jian
    Ng, Seik Weng
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : O794 - U2331
  • [2] Diphenyl 3,6-bis(4-chlorophenyl)-1,2-dihydro-1,2,4,5-tetrazine-1,2-dicarboxylate
    Zhong, GX
    Lv, LP
    Rao, GW
    Hu, WX
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2005, 61 : O1552 - O1553
  • [3] Bis(benzylaminium) 4,5-dichlorobenzene-1,2-dicarboxylate monohydrate
    Smith, Graham
    Wermuth, Urs D.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : O1928 - +
  • [4] Excited state proton transfer in 3,6-bis(4,5-dihydroxyoxazo-2-yl)benzene-1,2-diol
    Enchev, Venelin
    Markova, Nadezhda
    Stoyanova, Malinka
    Petrov, Petar
    Rogozherov, Marin
    Kuchukova, Nadya
    Timtcheva, Ilijana
    Monev, Valentin
    Angelova, Silvia
    Spassova, Milena
    CHEMICAL PHYSICS LETTERS, 2013, 563 : 43 - 49
  • [5] Dipropyl 3,6-bis(4-chlorophenyl)-1,2-dihydro-1,2,4,5-tetrazine-1,2-dicarboxylate
    Rao, GW
    Hu, WX
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2005, 61 : O2102 - O2103
  • [6] Synthesis and crystal structure of diethyl 3,6-diphenyl-1,2-dihydro-1,2,4,5-tetrazine-1,2-dicarboxylate
    Rao, GW
    Hu, WX
    CHINESE JOURNAL OF ORGANIC CHEMISTRY, 2004, 24 (12) : 1622 - 1625
  • [7] Synthesis and structure of bis(cyclohexylmethyl) 3,6-bis(4-chlorophenyl)-1,2,4,5-tetrazine-1,2-dicarboxylate
    Zhang, Shu
    Rao, Guo-Wu
    Mao, Xiao-Guang
    Hu, Wei-Xiao
    JOURNAL OF CHEMICAL RESEARCH, 2011, (05) : 275 - 277
  • [8] Bis[μ-(hydrogen benzene-1,2-dicarboxylato)-O:O′]bis[bis(1,10-phenanthroline-N,N′)cobalt(II)] bis(hydrogen benzene-1,2-dicarboxylate) dihydrate
    Poleti, D
    Karanovic, L
    Bogdanovic, GA
    Spasojevic-de Biré, A
    ACTA CRYSTALLOGRAPHICA SECTION C-STRUCTURAL CHEMISTRY, 1999, 55 : 2061 - 2063
  • [9] Bis[diethyl(hydroxy)ammonium] benzene-1,4-dicarboxylate
    Xie, De-Ming
    Chen, Chun-Xiao
    Chen, Hai-Xiang
    Wang, Hai-Bin
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : O2074 - U1702
  • [10] Dimethyl 4,5-dichlorobenzene-1,2-dicarboxylate
    Sun, Yongling
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : O834 - U2941
12345