[Ru(CO)(CH3CO2)(tpa)]ClO4•C6H5CH3 (tpa = tris(2-pyridylmethyl)amine), the first ruthenium carbonyl complex of tpa

被引：4

作者：

Xu, L ^{[1
]}

Sasaki, Y ^{[1
]}

机构：

[1] Hokkaido Univ, Grad Sch Sci, Div Chem, Kita Ku, Sapporo, Hokkaido 0600810, Japan

来源：

INORGANIC CHEMISTRY COMMUNICATIONS | 1999年 / 2卷 / 04期

关键词：

ruthenium complexes; polypyridyl complexes; carboxylate complexes; carbonyl complexes;

D O I：

10.1016/S1387-7003(99)00026-X

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

The reaction of dodecacarbonyltriruthenium with tris(2-pyridylmethyl) ammonium perchlorate (tpa . 3HClO(4)), in the presence of acetic acid, afforded a new ruthenium complex of tpa, [Ru(CO)(CH3CO2)(tpa)]ClO4. C6H5CH3 (1). Compound 1 has been characterized by X-ray structural analysis, IR and H-1 NMR spectra. (C) 1999 Elsevier Science S.A. All rights reserved.

引用

页码：121 / 123

页数：3

共 50 条

[31] Syntheses and characterization of η5-cyclopentadienyl and η5-indenyl ruthenium(II) complexes of arylazoimidazoles:: The molecular structure of the complex [(η5-C5H5)Ru(PPh3)(C6H5-N=N-C3H3N2)]+
Govindaswamy, P
Sinha, C
Kollipara, MR
JOURNAL OF ORGANOMETALLIC CHEMISTRY, 2005, 690 (14) : 3465 - 3473
[32] Crystal and Molecular Structure of Binuclear Technetium Carbonyl Chloride Complexes [99TcCl(CO)3(C5H8O2)]2 (C5H8O2 = Acetylacetone) and [99TcCl(CO)4]2
Sidorenko, G. V.
Miroslavov, A. E.
Gurzhiy, V. V.
Kochergina, A. R.
Sakhonenkova, A. P.
Tyupina, M. Yu.
Chistyi, L. S.
Pechertseva, E. A.
RADIOCHEMISTRY, 2024, 66 (04) : 405 - 415
[33] Heats of reaction of HMo(CO)(3)(C(5)R(5)) (R=H, CH3) with diphenyldisulfide and of formation of the clusters [PhSMo(CO)(x)(C5H5)](2), x=1,2. Thermodynamic study of molybdenum-sulfur bond strengths
Mukerjee, SL
Gonzalez, AA
Nolan, SP
Ju, TD
Lang, RF
Hoff, CD
INORGANICA CHIMICA ACTA, 1995, 240 (1-2) : 175 - 182
[34] A novel octa-substituted iridium carbonyl derivative containing the dehydrogenated dppf ligand (dppf=Fe(C5H4PPh2)(2)): synthesis and crystal structure of [H4Ir4(CO)(4){Fe(C5H3PPh2)(C5H4P(Ph)C6H4)}(2)]
Ueng, CH
Lu, SM
INORGANICA CHIMICA ACTA, 1997, 262 (02) : 113 - 115
[35] One-step syntheses of Ph(3)P-substituted selenido carbonyl iron and ruthenium clusters .2. Crystals structures Fe-2(mu(2)-Se-2)(CO)(6-n)(PPh(3))n (n=1 or 2), Fe-3(mu(3)-Se)(2)(CO)(8)(PPh(3)) and Ru-4(mu(4)-se)(2)(mu-CO)(2)(CO)(8)(PPh(3)), and HPLC behaviour of the iron derivatives
Baistrocchi, P
Careri, M
Cauzzi, D
Graiff, C
Lanfranchi, M
Manini, P
Predieri, G
Tiripicchio, A
INORGANICA CHIMICA ACTA, 1996, 252 (1-2) : 367 - 374
[36] First Examples of Electrophilic Addition to a Fe2Q Face of [Fe3(μ3-Q)(CO)9]2− (Q=Se, Te)—Synthesis and Characterisation of [MFe3(μ4-Q)(CO)9Cp*] and [IrFe2(μ3-Q)(CO)7Cp*] (M=Rh, Ir; Cp*=η5-C5(CH3)5)
Sergei N. Konchenko
Nikolai A. Pushkarevsky
Manfred Scheer
Journal of Cluster Science, 2003, 14 : 299 - 312
[37] Migratory insertion reaction in alkenyl ruthenium(II) complexes containing a trifluoroacetate ligand.: X-ray structure of the Ru(η2-O2CCF3) (η1-O=CCH=CH(t)BU) (CO) (PPh3)2 complex
Matas, L
Muniente, J
Ros, J
Alvarez-Larena, A
Piniella, JF
INORGANIC CHEMISTRY COMMUNICATIONS, 1999, 2 (08) : 364 - 367
[38] AN ASYMMETRIC HOMODINUCLEAR COMPLEX CONTAINING THE MU-OXO-BIS(MU-CARBOXYLATO)DIRUTHENIUM(III) CORE - X-RAY STRUCTURE OF [RU2O(O2CC6H4-P-OME)(3)(EN)(PPH(3))(2)](CLO4)CENTER-DOT-3CHCL(3)
SYAMALA, A
NETHAJI, M
CHAKRAVARTY, AR
INORGANICA CHIMICA ACTA, 1995, 229 (1-2) : 33 - 38
[39] First examples of electrophilic addition to a Fe2Q face of [Fe3(μ3-Q)(CO)9]2- (Q=Se, Te) -: Synthesis and characterisation of [MFe3(μ4-Q)(CO)9Cp*] and [IrFe2(μ3-Q)(CO)7Cp*] (M=Rh, Ir; Cp*=η5-C5(CH3)5)
Konchenko, SN
Pushkarevsky, NA
Scheer, M
JOURNAL OF CLUSTER SCIENCE, 2003, 14 (03) : 299 - 312
[40] Thermolysis of Ru3(CO)10(dppb): Activation of C-H and P-Ph bonds in PPh2P(CH2)4PPh2 (dppb=1,4-bis(diphenylphosphino)butane)
bin Shawkataly, Omar
Sirat, Siti Syaida
Rosli, Mohd Mustaqim
Razak, Ibrahim Abdul
POLYHEDRON, 2016, 117 : 193 - 201

← 1 2 3 4 5 →