Qualitative and quantitative analysis of Swertia herbs by high performance liquid chromatography-diode array detector-mass spectrometry (HPLC-DAD-MS)

被引：20

作者：

Wang, Zhigang ^{[1
]}

Ma, Chaomei ^{[1
]}

Tang, Shuhan ^{[1
]}

Xiao, Huai ^{[2
]}

Kakiuchi, Nobuko ^{[3
]}

Kida, Hiroaki ^{[4
]}

Hattori, Masao ^{[1
]}

机构：

[1] Toyama Univ, Inst Natl Med, Div Metab Engn, Toyama 9300194, Japan

[2] Dali Univ, Dept Pharm, Dali, Yunnan Province 671000, Japan

[3] Kanazawa Univ, Grad Sch Nat Sci & Technol, Kanazawa, Ishikawa 9201192, Japan

[4] ALPS Pharmaceut Ind Co Ltd, Gifu 5094241, Japan

来源：

CHEMICAL & PHARMACEUTICAL BULLETIN | 2008年 / 56卷 / 04期

关键词：

Swertia herb; liquid chromatography-mass spectrometry; quality control; quantitative determination;

D O I：

10.1248/cpb.56.485

中图分类号：

R914 [药物化学];

学科分类号：

100701 ;

摘要：

We evaluated the composition of Swertia herbs using high performance liquid chromatography-diode array detector-mass spectrometry (HPLC-DAD-MS). Eleven peaks of 6 species were unequivocally identified by comparing their retention times, UV spectra, on-line electrospray ionization mass (EST-MS) spectra, and collision-induced dissociation mass spectrometry/mass spectrometry (CID-MS/MS) data with those of authentic compounds. We adopted wavelengths of 254 nm, 340 nm and 230 urn to simultaneously determine these I I compounds. By comparing the overall DAD and total ion current (TIC) profiles of various samples, the 6 species were differentiated in terms of the occurrence and/or relative concentrations of the eleven compounds. Our novel validated HPLC-DAD-MS method not only facilitates quality control and identification of Swertia herbs, but is also applicable to systematic investigations of the distribution of secoiridoids, flavonoids, and xanthones in the genus Swertia.

引用

页码：485 / 490

页数：6

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