Qualitative TLC determination of some polycyclic aromatic hydrocarbons in sugar-beet

被引：9
|
作者：
Loncar, ES [1 ]
Kolarov, LA [1 ]
Malbasa, RV [1 ]
Skrbic, BD [1 ]
机构：
[1] Univ Novi Sad, Fac Technol, Novi Sad 21000, Serbia Monteneg
来源：
JOURNAL OF THE SERBIAN CHEMICAL SOCIETY | 2005年 / 70卷 / 10期
关键词：
PAHs; sugar-beet; cyclohexane extracts; TLC; silica gel;
D O I：
10.2298/JSC0510237L
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
The presence of polycyclic or polynuclear aromatic hydrocarbons (PAHs) were investigated in sugar-beet from a local sugar factory in the district of Vojvodina. The sugar-beet was cultivated on areas near roads with intensive traffic. The procedure for the preparation and determination of these compounds included saponification of the sample, several liquid-liquid extraction systems and a silica gel column clean-tip. The purified sample solution was analysed by thin layer chromatography (TLC) on silica gel with cyclohexane as the developing solvent. Benzo(b)fluoranthene and benzo(a)anthracene and/or benzo(a)pyrene were detected at concentrations greater than the allowed limits in food.
引用
收藏
页码：1237 / 1242
页数：6
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