Synthesis and Characterization of NiFe2O4 Magnetic Nanoparticles for Magnetic Resonance Imaging Application

被引:2
作者
Sitthichai, Sudarat [1 ]
Junploy, Patcharanan [2 ]
Thongtem, Titipun [3 ,4 ]
Pilapong, Chalermchai [5 ]
Phuruangrat, Anukorn [6 ]
Thongtem, Somchai [1 ,3 ]
机构
[1] Chiang Mai Univ, Fac Sci, Dept Phys & Mat Sci, Chiang Mai 50200, Thailand
[2] Chiang Mai Rajabhat Univ, Fac Sci & Technol, Dept Chem, Chiang Mai 50300, Thailand
[3] Chiang Mai Univ, Fac Sci, Mat Sci Res Ctr, Chiang Mai 50200, Thailand
[4] Chiang Mai Univ, Dept Chem, Fac Sci, Chiang Mai 50200, Thailand
[5] Chiang Mai Univ, Fac Associated Med Sci, Ctr Excellence Mol Imaging CEMI, Dept Radiol Technol, Chiang Mai 50200, Thailand
[6] Prince Songkla Univ, Fac Sci, Div Phys Sci, Hat Yai 90112, Songkhla, Thailand
关键词
NiFe2O4 magnetic nanoparticles; XRD; TEM; XPS; OXIDE; PHOTOCATALYST; BLUE;
D O I
10.1142/S0219581X21500472
中图分类号
TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
NiFe2O4 magnetic nanoparticles (MNPs) were synthesized by co-precipitation of iron (III) chloride hexahydrate and nickel (II) chloride hexahydrate in the solution containing 45% hydrazine at 80(circle)C. Phase, morphology, oxidation state and magnetic properties were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), selected area electron diffraction (SAED), X-ray photoelectron spectroscopy (XPS) and vibrating sample magnetometry (VSM). In this research, pure NiFe2O4 MNPs synthesized in the solution with the pH of 10 with saturation magnetization of 49.839emu/g were detected and were able to be used for magnetic resonance imaging (MRI) application with very high contrast.
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页数:7
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