A novel benzofuro-(2, 3-c)-7′-chromene from Cassia sieberiana

被引:0
|
作者
Nvau, John Barnabas [1 ]
Ajibade, Sunday Olugbenga [2 ]
Gray, Alexander Irvine [3 ]
Igoli, John Ogbaji [3 ,4 ]
机构
[1] Plateau State Univ, Dept Chem, Bokkos, Nigeria
[2] Redeemers Univ, Dept Chem Sci, Ede, Osun State, Nigeria
[3] Univ Strathclyde, Strathclyde Inst Pharm & Biomed Sci, Glasgow, Lanark, Scotland
[4] Univ Agr, Dept Chem, Makurdi, Nigeria
关键词
Lupeol; epiafzelechin; Cassia sieberiana; chromatography; benzofurochromene; Nigeria;
D O I
10.1080/14786419.2020.1719483
中图分类号
O69 [应用化学];
学科分类号
081704 ;
摘要
The stem bark of Cassia sieberiana was extracted with methanol and the methanol extract partitioned with chloroform. Column chromatography of the chloroform fraction over silica gel yielded a novel benzofurochromene [2-(4-hydroxylphenyl)-7'-1, 2-dihydroxy-1-phenylpropyl)-4', 6'-dihydroxy [1] phenylbenzofuro (2, 3-c)-7'-chromene], lupeol and epiafzelechin. Their structures determined by Nuclear Magnetic resonance and mass spectrometry.
引用
收藏
页码:3619 / 3624
页数:6
相关论文
共 50 条
  • [31] Dramatic effects of the substituents on the solid-state fluorescence properties of structural isomers of novel benzofuro[2,3-c]oxazolocarbazole-type fluorophores
    Ooyama, Yousuke
    Harima, Yutaka
    CHEMISTRY LETTERS, 2006, 35 (08) : 902 - 903
  • [32] Novel heteroaromatic system: The thieno[3′,4′:4,5]thieno[2,3-c]pyrylium cation [7]
    Tolkunov, S.V.
    Dulenko, V.I.
    Chemistry of Heterocyclic Compounds, 2001, 37 (06) : 787 - 788
  • [33] Synthesis of benzofuro[2,3-c]pyridines via a one-pot three-component reaction
    Hu, Jiaxing
    Deng, Zhihong
    Zhang, Xueqiong
    Zhang, Fanglin
    Zheng, Hua
    ORGANIC & BIOMOLECULAR CHEMISTRY, 2014, 12 (27) : 4885 - 4889
  • [34] Synthesis and Molluscicidal Activity of Some Newly Substituted Chromene and Pyrano[2,3-c]pyrazole Derivatives
    Abdelrazek, Fathy M.
    Metwally, Nadia H.
    Sobhy, Nehal A.
    AFINIDAD, 2008, 65 (538) : 482 - 487
  • [35] REACTIONS WITH NITRILES - A NOVEL SYNTHESIS OF FURO[2,3-C]PYRAZOLES AND PYRANO[2,3-C]PYRAZOLES
    AZIZ, SI
    ABDALLAH, SO
    IBRAHIM, NS
    HETEROCYCLES, 1984, 22 (11) : 2523 - 2527
  • [36] A NOVEL SYNTHESIS OF STEROIDAL[2,3-C]THIOPHENES
    KANEKO, H
    YAMATO, Y
    KUROKAWA, M
    CHEMICAL & PHARMACEUTICAL BULLETIN, 1968, 16 (07) : 1200 - +
  • [37] A novel synthesis of thieno[2,3-c]pyrazole
    Wang, ZW
    Li, ZM
    Ren, J
    Chen, HS
    SYNTHETIC COMMUNICATIONS, 1999, 29 (13) : 2355 - 2359
  • [38] An Eco-friendly Synthesis of Some Novel 4-methyl-4-hetaryl Chromene and Pyrano[2,3-c]pyrazole Derivatives
    Abdelrazek, Fathy M.
    Metz, Peter
    Jaeger, Anne
    Metwally, Nadia H.
    JOURNAL OF HETEROCYCLIC CHEMISTRY, 2017, 54 (04) : 2313 - 2318
  • [39] ORGN 485-Synthesis of benzofuro[2,3-c]pyridinols: Probes for narcotic receptor mediated phenomena.
    Iyer, Malliga R.
    Jacobson, Arthur E.
    Rice, Kenner C.
    ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 2008, 236
  • [40] Triphosgene in heterocyclic chemistry, novel synthesis of pyrazolo (2, 3-c) quinazoline from 2-acetamido acetophenone hydrazone
    Al-Saad, MA
    Jum'h, AAM
    ASIAN JOURNAL OF CHEMISTRY, 2000, 12 (03) : 655 - 658