The influence of ethylene glycol on the preparation of K2SnSi3O9•H2O

被引：0
|
作者：
Lin, Zhi [1 ]
机构：
[1] Univ Aveiro, Dept Chem, CICECO, P-3810193 Aveiro, Portugal
来源：
ZEOLITES AND RELATED MATERIALS: TRENDS, TARGETS AND CHALLENGES, PROCEEDINGS OF THE 4TH INTERNATIONAL FEZA CONFERENCE | 2008年 / 174卷
关键词：
Silicate; stannosilicate; solvothermal synthesis;
D O I：
暂无
中图分类号：
O69 [应用化学];
学科分类号：
081704 ;
摘要：
The influence of ethylene glycol (EG) on the preparation of K(2)SnSi(3)O(9)center dot H(2)O (AV-6) was studied in this work. The EG content clearly changes the synthesis process. Although the morphology of the samples is similar, the products are mixtures containing AV-6, AV-7 (K(2)SnSi(3)O(9)center dot H(2)O) and AV-11 (K(4)Sn(2)Si(6)O(18)). At high EG content, nano crystal of Sn-AV-11, instead of AV-6, is crystallized from the system. The samples were characterized by powder XRD, SEM, solid-state (29)Si MAS NMR spectroscopy and thermogravimetric (TG) analysis.
引用
收藏
页码：301 / 304
页数：4
相关论文
共 50 条
  • [1] The influence of ethylene glycol on the preparation of K2SnSi3O9·H2O
    Lin, Zhi
    Studies in Surface Science and Catalysis, 2008, 174 (0A) : 301 - 304
  • [2] Compositions, Densities, and Refractive Indices for the Ternary Systems Ethylene Glycol + NaCl + H2O, Ethylene Glycol + KCl + H2O, Ethylene Glycol + RbCl + H2O, and Ethylene Glycol + CsCl + H2O at 298.15 K
    Zhou, Yanhong
    Li, Shu'ni
    Zhai, Quanguo
    Jiang, Yucheng
    Hu, Mancheng
    JOURNAL OF CHEMICAL AND ENGINEERING DATA, 2010, 55 (03): : 1289 - 1294
  • [3] K2TiSi3O9•H2O
    Zou, XD
    Dadachov, MS
    ACTA CRYSTALLOGRAPHICA SECTION C-STRUCTURAL CHEMISTRY, 2000, 56 : 738 - 739
  • [4] PREPARATION AND STRUCTURE OF K2SNS3 2 H2O
    SCHIWY, W
    BLUTAU, C
    GATHJE, D
    KREBS, B
    ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE, 1975, 412 (01): : 1 - 10
  • [5] HYDRATED PHASES IN THE V2O5-K2O-SO3-H2O SYSTEM - PREPARATION AND STRUCTURES OF K[VO2(SO4)(H2O)] AND K[VO2(SO4)(H2O)2].H2O
    RICHTER, KL
    MATTES, R
    INORGANIC CHEMISTRY, 1991, 30 (23) : 4367 - 4369
  • [6] THE SIMPLE CLUSTERS (H3O+)(H2O)1, (H3O+)(H2O)2, (H3O+)(H2O)3
    SCHAEFER, HF
    ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 1985, 189 (APR-): : 103 - PHYS
  • [7] Base fluid and temperature effects on the heat transfer characteristics of SiC in ethylene glycol/H2O and H2O nanofluids
    Timofeeva, Elena V.
    Yu, Wenhua
    France, David M.
    Singh, Dileep
    Routbort, Jules L.
    JOURNAL OF APPLIED PHYSICS, 2011, 109 (01)
  • [8] [Yb(H2O)8][Cd3Cl9(H2O)]•6H2O
    Yahyaoui, Samia
    Naili, Houcine
    Ben Hassen, Rached
    Donadieu, Bruno
    Daran, Jean Claude
    Ben Salah, Abdelhamid
    ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES, 2004, 60 : S279 - S279
  • [9] [Yb(H2O)8][Cd3Cl9(H2O)]•6H2O
    Yahyaoui, S
    Ben Hassen, R
    Donnadieu, B
    Daran, JC
    Ben Salah, A
    ACTA CRYSTALLOGRAPHICA SECTION C-STRUCTURAL CHEMISTRY, 2003, 59 : I109 - I111
  • [10] ON THE REPORTED PREPARATION OF [MO2O4(ACAC)2(H2O)2] . H2O
    CHAKRAVORTI, MC
    BANDYOPADHYAY, D
    TRANSITION METAL CHEMISTRY, 1985, 10 (08) : 319 - 319
12345