Microwave-Assisted Synthesis of Some New Mixed Ligand Ni(II) Complexes Its Characterization and Its Antimicrobial Study

被引:1
|
作者
Pawara, Jitendra M. [1 ]
Patil, Sunil S. [1 ]
机构
[1] Changu Kana Thakur Arts Commerce & Sci Coll Auton, Dept Chem, New Panvel, Maharashtra, India
关键词
Ni(II) complexes; 2-amino-6-methyl pyrimidine-4-ol; amino acids; microwave-assisted; antimicrobial activity; CRYSTAL-STRUCTURE; METAL-COMPLEXES; AMINO-ACIDS; SPECTRA; DIOXOURANIUM(VI); ANTIFUNGAL; COPPER(II); NICKEL(II); CO(II);
D O I
10.9734/JPRI/2021/v33i31B31700
中图分类号
R9 [药学];
学科分类号
1007 ;
摘要
Nickel(II) complexes of the type [Ni(P)(L)center dot 2H(2)O] has been synthesized by using 2-amino-6-methyl pyrimidine-4-ol (HP) and amino acids (HL). Complexes synthesized by conventional as well as microwave methods. Results indicate that complexes synthesized by the microwave method are more efficient than the conventional method. In the microwave method preparation time is short (47 min.) compared to the conventional method (45 min.). Moreover, the microwave Assisted method gives a very high yield (90%) of the complexes. The microwave method used for the synthesis of the complexes has been found easier, convenient and eco-friendly. Complexes have been characterized by FTIR, Elemental analysis, Gouy experiment, Thermogravimetric Analysis (TGA) and Differential Thermal Analysis (DTA). Complexes have shown significant antimicrobial activity.
引用
收藏
页码:143 / 152
页数:10
相关论文
共 50 条
  • [41] Design, synthesis and characterization of macrocyclic ligand based transition metal complexes of Ni(II), Cu(II) and Co(II) with their antimicrobial and antioxidant evaluation
    Gull, Parveez
    Malik, Manzoor Ahmad
    Dar, Ovas Ahmad
    Hashmi, Athar Adil
    JOURNAL OF MOLECULAR STRUCTURE, 2017, 1134 : 734 - 741
  • [42] Synthesis, characterization, antiproliferative of pyrimidine based ligand and its Ni(II) and Pd(II) complexes and effectiveness of electroporation
    Alkis, Mehmet Esref
    Buldurun, Kenan
    Turan, Nevin
    Alan, Yusuf
    Yilmaz, Unzile Kelestemur
    Mantarci, Asim
    JOURNAL OF BIOMOLECULAR STRUCTURE & DYNAMICS, 2022, 40 (09) : 4073 - 4083
  • [43] Synthesis, characterization and thermal study of some transition metal complexes of an asymmetrical tetradentate Schiff base ligand
    Munde, Achut S.
    Jagdale, Amarnath N.
    Jadhav, Sarika M.
    Chondhekar, Trimbak K.
    JOURNAL OF THE SERBIAN CHEMICAL SOCIETY, 2010, 75 (03) : 349 - 359
  • [44] Synthesis, characterization and antimicrobial screening of a novel organylborate ligand, potassium hydro(phthalyl)(salicylyl)borate and its Co(II), Ni(II), and Cu(II) complexes
    Sheikh, Rayees Ahmad
    Shreaz, Sheikh
    Sharma, Guruaribam Shashikumar
    Khan, Luqman Ahmad
    Hashmi, Athar Adil
    JOURNAL OF SAUDI CHEMICAL SOCIETY, 2012, 16 (04) : 353 - 361
  • [45] Microwave-Assisted Synthesis and Spectral Characterization of Biological Activity Heterocyclic Thiosemicarbazone and Its Organometallic Derivatives
    Zayed, Mohie E. M.
    JOURNAL OF HETEROCYCLIC CHEMISTRY, 2019, 56 (01) : 32 - 37
  • [46] Template synthesis, characterization and antimicrobial activity of some new complexes with isonicotinoyl hydrazone ligands
    Mitu, Liviu
    Raman, Natarajan
    Kriza, Angela
    Stanica, Nicolae
    Dianu, Mariana
    JOURNAL OF THE SERBIAN CHEMICAL SOCIETY, 2009, 74 (10) : 1075 - 1084
  • [47] Synthesis, Characterization, and Spectroscopic Properties of a Symmetrical Schiff Base Ligand and its Bimetallic Complexes
    Bayrakci, Mevlut
    Ertul, Seref
    Bas, Salih Zeki
    Demir, Ibrahim
    SYNTHESIS AND REACTIVITY IN INORGANIC METAL-ORGANIC AND NANO-METAL CHEMISTRY, 2011, 41 (05) : 484 - 490
  • [48] Pyrimidine hydrazide ligand and its metal complexes: synthesis, characterization, and antimicrobial activities
    Saeed, S. El-Sayed
    Alomari, Budoor A.
    Al-Hakimi, Ahmed N.
    Abd El-Hady, M. M.
    Alnawmasi, Jawza Sh
    Elganzory, Hussein H.
    El-Sayed, Wael A.
    EGYPTIAN JOURNAL OF CHEMISTRY, 2023, 66 (05): : 315 - 330
  • [49] Synthesis, Spectroscopic Characterization, and Antifungal Activity of Some Mixed Ligand Complexes of Zn(II), Cd(II), and Hg(II)
    Sharma, Renu
    Nagar, Meena
    PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS, 2010, 185 (07) : 1526 - 1535
  • [50] Antimicrobial and anticancer activities of Schiff base ligand and its transition metal mixed ligand complexes with heterocyclic base
    Abd El-Halim, H. F.
    Mohamed, Gehad G.
    Anwar, Mahmoud N.
    APPLIED ORGANOMETALLIC CHEMISTRY, 2018, 32 (01)