Preparation of nanostructured high-temperature TZM alloy by mechanical alloying and sintering

被引:57
作者
Ahmadi, E. [1 ]
Malekzadeh, M. [1 ]
Sadrnezhaad, S. K. [1 ,2 ]
机构
[1] Mat & Energy Res Ctr, Tehran, Iran
[2] Sharif Univ Technol, Ctr Excellence Adv Proc Prod Mat, Dept Mat Sci & Engn, Tehran, Iran
关键词
TZM; Sintering; Mechanical alloying; Nanostructure; TENSILE PROPERTIES; MOLYBDENUM; CREEP; DISPERSION; CARBON; LCAC; MO; SI;
D O I
10.1016/j.ijrmhm.2010.09.003
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Mechanical milling proceeded by sintering was used to synthesize nanostructured temperature-resistant TZM alloy Milling under Ar for different times (1 2 3 4 10 15 20 25 and 30 h) and sintering at 1500 1600 and 1700 C for 30 45 60 and 90 min resulted in increasing of low energy grain boundaries (LEGBs) and dispersion of TiC and ZrC with a size of similar to 65 nm in the matrix near LEGBs Morphology and grain size of the products were determined from scanning electron microscope (SEM) images and X ray diffraction (XRD) patterns almost precisely Optimum density of nanostructured TZM alloy similar to 9 95 +/- 0 01 g/cm(3) was achieved by sintering at 1700 C for 90 min (C) 2010 Elsevier Ltd All rights reserved
引用
收藏
页码:141 / 145
页数:5
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