One-pot synthesis of supported-nanoparticle materials in ionic liquid solvents

被引：13

作者：

Dash, Priyabrat ^{[1
]}

Scott, Robert W. J. ^{[1
]}

机构：

[1] Univ Saskatchewan, Dept Chem, Saskatoon, SK S7N 0W0, Canada

来源：

MATERIALS LETTERS | 2011年 / 65卷 / 01期

基金：

加拿大自然科学与工程研究理事会;

关键词：

Ionic liquids; Nanoparticles; Supported nanoparticle materials; CO OXIDATION; CATALYSTS; HYDROGENATION;

D O I：

10.1016/j.matlet.2010.09.031

中图分类号：

T [工业技术];

学科分类号：

08 ;

摘要：

Highly porous supported-nanoparticle materials were synthesized by a rational method involving the encapsulation of poly(vinylpyrrolidone) (PVP) stabilized Au nanoparticles Into Mania xerogels employing room temperature ionic liquids (1 butyl-3 methylimidazolium hexaflurophosphate [BMIM]PF6) as a medium followed by solvent extraction of the ionic liquid and calcination of the materials The materials were thoroughly characterized by TEM nitrogen adsorption-desorption isotherms and XRD After calculations at 350 C the Au-titania system resulted in the formation of a highly mesoporous materials with BET surface areas of 200 m(2)/g and average pore sizes of 3-5 nm These materials can find potential applications in catalysis and photocatalysis (C) 2010 Elsevier B V All rights reserved

引用

页码：7 / 9

页数：3

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