Rietveld refinement of ternary compound Gd117Fe52Ge112

被引:7
作者
He, Wei [1 ]
Zhang, Jiliang [1 ]
Zeng, Lingmin [1 ]
机构
[1] Guangxi Univ, Dept Phys, Minist Educ, Key Lab Nonferrous Metal Mat & New Proc Technol, Nanning 530004, Peoples R China
关键词
Gd117Fe52Ge112; crystal structure; Rietveld method; X-ray diffraction data;
D O I
10.1154/1.2793073
中图分类号
TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
A new ternary compound Gd117Fe52Ge112 has been successfully synthesized and studied by means of X-ray powder diffraction technique. Gd117Fe52Ge112 crystallizes in a cubic Tb117Fe52Ge112-type structure with space group Fm (3) over barm(#225) and lattice parameter a=28.7680(1) angstrom. Crystal structure of Gd117Fe52Ge112 has been successfully refined using the Rietveld method from X-ray diffraction data. The R-factors for the Rietveld refinement are R-p=0.099 and R-wp=0.128. X-ray powder diffraction data with the figure of merit F-30 of 80.4(30) are also reported. (C) 2007 International Centre for Diffraction Data.
引用
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页码:312 / 315
页数:4
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