Optical And X-ray Photoelectron Spectroscopy Studies Of α-Al2O3

被引:13
作者
Prakash, Ram [1 ]
Kumar, Sandeep [1 ]
Kumar, Vinay [1 ]
Choudhary, R. J. [2 ]
Phase, D. M. [2 ]
机构
[1] Shri Mata Vaishno Devi Univ, Sch Phys, Katra 182320, Jammu & Kashmir, India
[2] UGC DAE Consortium Sci Res, Indore 452001, Madhya Pradesh, India
来源
DAE SOLID STATE PHYSICS SYMPOSIUM 2015 | 2016年 / 1731卷
关键词
Combustion Synthesis; XRD; XPS; ALUMINA CERAMICS;
D O I
10.1063/1.4947751
中图分类号
O59 [应用物理学];
学科分类号
摘要
alpha-Al2O3 powder sample was synthesized at 550 degrees C via solution combustion synthesis (SCS) method using urea as an organic fuel. The sample was characterized by X-ray diffraction (XRD), Optical spectroscopy and X-ray photoelectron spectroscopy (XPS) without any further thermal treatment. XRD study reveals that the powder crystallized directly in the hexagons alpha-Al2O3 phase. A band gap of 5.7 eV was estimated using diffuse reflectance spectra. For surface investigation X-ray photo electron spectroscopy (XPS) was carried out. The XPS survey scan study of alpha-Al2O3 powder reveals that the sample is free from impurity. The core levels of Al-2s and O-1s are also reported.
引用
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页数:3
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