transmission electron microscopy;
visible spectra;
surface plasmon resonance;
nanofabrication;
ultraviolet spectra;
field emission electron microscopy;
reduction (chemical);
nanocomposites;
microorganisms;
nanoparticles;
dyes;
silver;
X-ray diffraction;
nanomedicine;
gold;
antibacterial activity;
electron diffraction;
infrared spectra;
particle size;
Fourier transform spectra;
scanning electron microscopy;
catalysis;
crystal growth from solution;
synthesised nanoparticles;
gold nanoparticles;
catalytic activities;
electron diffraction patterns;
antimicrobial activities;
antioxidant activities;
transmission electron microscopy images;
2;
2-diphenyl-1-picrylhydrazyl assay;
Synedrella nodiflora;
UV-Vis spectrum;
silver nanoparticles;
biofabrication;
Fourier transform infrared spectroscopy;
face-centred cubic geometry;
area electron diffraction patterns;
pathogenic strains;
agar well diffusion method;
anthropogenic pollutant dyes;
Congo red;
eosin Y;
wavelength;
413;
0;
nm;
535;
Au;
Ag;
MICROWAVE-ASSISTED GREEN;
LEAF EXTRACT;
STRUCTURAL-CHARACTERIZATION;
ESCHERICHIA-COLI;
ANTIBACTERIAL;
BIOSYNTHESIS;
REDUCTION;
DEGRADATION;
ANTICANCER;
OXIDATION;
D O I:
10.1049/iet-nbt.2017.0311
中图分类号:
Q5 [生物化学];
学科分类号:
071010 ;
081704 ;
摘要:
The present work is emphasised on the bio-fabrication of silver and gold nanoparticles in a single step by a microwave-assisted method using the leaf extract of Synedrella nodiflora as both reducing and stabilising agent. The synthesised nanoparticles are highly stable and show surface plasmon resonance peak at 413 and 535nm, respectively, for silver and gold nanoparticles in UV-Vis spectrum. The functional group responsible for the reduction of metal ions were obtained from Fourier transform infrared spectroscopy. The crystalline nature of nanoparticles with face-centred cubic geometry was confirmed by the X-ray diffraction and selected area electron diffraction patterns. The morphology and sizes of the silver and gold nanoparticles were obtained from transmission electron microscopy images. The nanoparticles exhibit effective antimicrobial activities against various pathogenic strains. These antimicrobial properties were analysed by employing agar well diffusion method. The nanoparticles show significant antioxidant properties, and it was determined using 2, 2-diphenyl-1-picrylhydrazyl assay. The nanoparticles also show potent catalytic activity in the degradation of anthropogenic pollutant dyes Congo red and eosin Y by excess NaBH4. Thus, the current study demonstrates the potential use of S. nodiflora as a reducing and stabilising agent for the synthesis of silver and gold nanoparticles and their relevance in the field of biomedicine and catalysis.
机构:
Jeonbuk Natl Univ, Coll Agr & Life Sci, Dept Food Sci & Technol, 567 Baekje Daero, Jeonju Si 54896, Jeollabuk Do, South Korea
Jeonbuk Natl Univ, Coll Agr & Life Sci, Dept Agr Convergence Technol, 567 Baekje Daero, Jeonju Si 54896, Jeollabuk Do, South KoreaJeonbuk Natl Univ, Coll Agr & Life Sci, Dept Food Sci & Technol, 567 Baekje Daero, Jeonju Si 54896, Jeollabuk Do, South Korea
Krishnaraj, Chandran
Kaliannagounder, Vignesh Krishnamoorthi
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机构:
Jeonbuk Natl Univ, Grad Sch, Dept Bionanotechnol & Bioconvergence Engn, 567 Baekje Daero, Jeonju Si 54896, Jeollabuk Do, South Korea
Jeonbuk Natl Univ, Grad Sch, Dept Bionanosyst Engn, 567 Baekje Daero, Jeonju Si 54896, Jeollabuk Do, South KoreaJeonbuk Natl Univ, Coll Agr & Life Sci, Dept Food Sci & Technol, 567 Baekje Daero, Jeonju Si 54896, Jeollabuk Do, South Korea
Kaliannagounder, Vignesh Krishnamoorthi
Rajan, Ramachandran
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机构:
Shandong Univ Technol, Sch Phys & Optoelect Engn, Lab Funct Mol & Mat, Zibo 255000, Shandong, Peoples R ChinaJeonbuk Natl Univ, Coll Agr & Life Sci, Dept Food Sci & Technol, 567 Baekje Daero, Jeonju Si 54896, Jeollabuk Do, South Korea
Rajan, Ramachandran
Ramesh, Thiyagarajan
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机构:
Prince Sattarn Bin Abdulaziz Univ, Coll Med, Dept Basic Med Sci, Al Kharj 11942, Saudi ArabiaJeonbuk Natl Univ, Coll Agr & Life Sci, Dept Food Sci & Technol, 567 Baekje Daero, Jeonju Si 54896, Jeollabuk Do, South Korea
Ramesh, Thiyagarajan
Kim, Cheol Sang
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机构:
Jeonbuk Natl Univ, Grad Sch, Dept Bionanotechnol & Bioconvergence Engn, 567 Baekje Daero, Jeonju Si 54896, Jeollabuk Do, South Korea
Jeonbuk Natl Univ, Grad Sch, Dept Bionanosyst Engn, 567 Baekje Daero, Jeonju Si 54896, Jeollabuk Do, South KoreaJeonbuk Natl Univ, Coll Agr & Life Sci, Dept Food Sci & Technol, 567 Baekje Daero, Jeonju Si 54896, Jeollabuk Do, South Korea
Kim, Cheol Sang
Park, Chan Hee
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Jeonbuk Natl Univ, Grad Sch, Dept Bionanotechnol & Bioconvergence Engn, 567 Baekje Daero, Jeonju Si 54896, Jeollabuk Do, South Korea
Jeonbuk Natl Univ, Mech Design Engn, 567 Baekje Daero, Jeonju Si 54896, Jeollabuk Do, South KoreaJeonbuk Natl Univ, Coll Agr & Life Sci, Dept Food Sci & Technol, 567 Baekje Daero, Jeonju Si 54896, Jeollabuk Do, South Korea
Park, Chan Hee
Liu, Bo
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机构:
Shandong Univ Technol, Sch Phys & Optoelect Engn, Lab Funct Mol & Mat, Zibo 255000, Shandong, Peoples R ChinaJeonbuk Natl Univ, Coll Agr & Life Sci, Dept Food Sci & Technol, 567 Baekje Daero, Jeonju Si 54896, Jeollabuk Do, South Korea