Orientation relationships and interface structure of α′-Cr nanoclusters embedded in α-Fe matrix after α-α′ demixing in neutron irradiated Oxide Dispersion Strengthened material

被引:27
作者
Ribis, J. [1 ]
Lozano-Perez, S. [2 ]
机构
[1] CEA Saclay, DEN DMN SRMA LA2M, CEA DEN DMN SRMA, F-91191 Gif Sur Yvette, France
[2] Univ Oxford, Dept Mat, Oxford OX1 3PH, England
关键词
Nuclear materials; Radiation damage; Nanoparticles; Interfaces; Electron microscopy; MARTENSITIC STEELS; FERRITIC STEELS; ALLOYS; PHASES;
D O I
10.1016/j.matlet.2012.01.115
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
A nanoscale characterization of neutron irradiated Oxide Dispersion Strengthened (ODS) alloys has been used to reveal the alpha-alpha' demixing and the population of (Y, Ti, O) nanoparticles. Multivariate statistical analysis (MSA) processed energy filtered transmission electron microscopy (EFTEM) efficiently reveals the location of all nanophases. The alpha-alpha' demixing did not only lead to the systematic formation of cube-on-cube semi-coherent Cr rich clusters but also to misfitting misoriented semi-coherent particles satisfying the orientation relationship [100](Cr)//[111](Fe) and [100](Cr)//[112](Fe). The misorientation angle between the semi-coherent directions < 110 >(Fe), and < 110 >(Cr) was found to be 17 degrees. (C) 2012 Elsevier B.V. All rights reserved.
引用
收藏
页码:143 / 146
页数:4
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