Preparation and characterization of electrospun Ag/polyacrylonitrile composite nanofibers

被引:14
作者
Bai, Jie [1 ,2 ]
Yang, Qingbiao [1 ]
Wang, Shan [2 ]
Li, Yaoxian [1 ]
机构
[1] Jilin Univ, Dept Chem, Changchun 130021, Peoples R China
[2] Inner Mongolia Univ Technol, Chem Engn Coll, Huhhote 010051, Peoples R China
关键词
Polyacrylonitrile (PAN); Electrospinning; Nanofibers; Ag Nanoparticles; Raman Spectroscopy; SILVER NANOPARTICLES; AG NANOPARTICLES; ELECTRIC-FIELD; FABRICATION; REDUCTION; FIBERS; GLASS;
D O I
10.1007/s11814-011-0006-8
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
Novel composite nanofibers consisting of Ag nanoparticles and polyacrylonitrile (PAN) were fabricated successfully. The Raman properties of these Ag/PAN nanofibers were studied at low temperatures, which showed good Raman characteristics. In the process, a PAN solution containing Ag ions was directly electrospun to obtain nanofiber films containing Ag ions, and the Ag ions of resulting composite nanofibers were reduced to Ag nanoparticles in N2H5OH aqueous solution. Then, we treated Ag/PAN composite nanofibers at 100 degrees C, 200 degrees C, 400 and 600 degrees C, respectively. The Ag/PAN nanocomposite film was characterized by scanning electron microscopy (SEM), X-ray diffraction (XRD) patterns and surface-enhanced Raman scattering (SERS) spectroscopy.
引用
收藏
页码:1761 / 1763
页数:3
相关论文
共 21 条
[1]  
Anton F., 1934, US patent, Patent No. [US1975504A, 1975504, 1975504A]
[2]   Silver-halide/organic-composite structures: Toward materials with multiple photographic functionalities [J].
Bringley, JF ;
Rajeswaran, M ;
Olson, LP ;
Liebert, NM .
JOURNAL OF SOLID STATE CHEMISTRY, 2005, 178 (10) :3074-3089
[3]   Novel nanocomposites and nanoceramics based on polymer nanofibers using electrospinning process - A review [J].
Chronakis, IS .
JOURNAL OF MATERIALS PROCESSING TECHNOLOGY, 2005, 167 (2-3) :283-293
[4]   An investigation of the surface-enhanced Raman scattering (SERS) effect from laser irradiation of Ag nanoparticles prepared by trisodium citrate reduction method [J].
Ding, Li-Ping ;
Fang, Yan .
APPLIED SURFACE SCIENCE, 2007, 253 (09) :4450-4455
[5]  
Formhals A, 1937, USA, Patent, Patent No. 2077373
[6]   Fabrication of collagen-coated biodegradable polymer nanofiber mesh and its potential for endothelial cells growth [J].
He, W ;
Ma, ZW ;
Yong, T ;
Teo, WE ;
Ramakrishna, S .
BIOMATERIALS, 2005, 26 (36) :7606-7615
[7]   A study on the preparation of poly(vinyl alcohol) nanofibers containing silver nanoparticles [J].
Jin, Wen-Ji ;
Jeon, Hyun Jeong ;
Kim, Jung Hyun ;
Youk, Ji Ho .
SYNTHETIC METALS, 2007, 157 (10-12) :454-459
[8]   Virus-based fabrication of micro- and nanofibers using electrospinning [J].
Lee, SW ;
Belcher, AM .
NANO LETTERS, 2004, 4 (03) :387-390
[9]   Photoinduced structural changes of silver nanoparticles on glass substrate in solution under an electric field [J].
Murakoshi, K ;
Tanaka, H ;
Sawai, Y ;
Nakato, Y .
JOURNAL OF PHYSICAL CHEMISTRY B, 2002, 106 (12) :3041-3045
[10]   A silver colloid produced by reduction with hydrazine as support for highly sensitive surface-enhanced Raman spectroscopy [J].
Nickel, U ;
Castell, AZ ;
Pöppl, K ;
Schneider, S .
LANGMUIR, 2000, 16 (23) :9087-9091