Crystal structure of two dimethyl 1,3-thiazolidinedicarboxylates obtained in thermal [2+3] cycloaddition of an azomethine ylide with 2,2,4,4-tetramethyl-3-thioxocyclobutanone

被引：1
作者：
Domagala, M
Malecka, M
Urbaniak, K
Mloston, G
Grabowski, SJ
机构：
[1] Univ Lodz, Dept Crystallog & Crystal Chem, PL-90236 Lodz, Poland
[2] Univ Lodz, Sect Heteroorgan Cpds, PL-90136 Lodz, Poland
来源：
STRUCTURAL CHEMISTRY | 2005年 / 16卷 / 01期
关键词：
crystal and molecular structure; C-H center dot center dot center dot S hydrogen bonds; the Bader theory; 2+3] cycloaddition;
D O I：
10.1007/s11224-005-1085-0
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
The crystal structures of dimethyl 2,2,4,4-tetramethyl-3-oxocyclobutane-1-spiro-5'-3',4'-diphenyl-(1,3)-thiazolidine-2',2'-dicarboxylate, C26H29NO5S for V, and dimethyl 3,4-diphenyl-5-isopropylidene-(1,3)-thiazolidine-2,2-dicarboxylate, C22H23NO4S for VI, have been solved. The 1,3-thiazolidine ring of compound V has got twisted conformation, while in compound VI this ring adopts envelope. In both structures short inter- and intramolecular contacts were found, which can be recognized as hydrogen bonds.
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页码：55 / 59
页数：5
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