Ethylene glycol assisted hydrothermal synthesis of flower-like and sphere-like ZnO

被引：2

作者：

Zou, Ke ^{[1
]}

Wu, Youshi ^{[1
]}

Zhao, Jinbo ^{[1
]}

Wu, Lili ^{[1
]}

机构：

[1] Shandong Univ, Key Lab Liquid Solid Struct Evolut & Proc Mat, Minist Educ, Jinan 250061, Peoples R China

来源：

MANUFACTURING PROCESSES AND SYSTEMS, PTS 1-2 | 2011年 / 148-149卷

关键词：

nanomaterials; luminescence; hydrothermal; ethylene glycol; GROWTH; NANOWIRES;

D O I：

10.4028/www.scientific.net/AMR.148-149.849

中图分类号：

T [工业技术];

学科分类号：

08 ;

摘要：

ZnO microsturctures with flower-like and sphere-like morphologies have been successfully synthesized in ethylene glycol (EG) -water solution at 160 degrees C through a hydrothermal method. The volume ratio of EG to H2O plays an important role on the morphology control of ZnO. CH3COONH4 and NaOH were used as hydroxide source as well as complexing agents. The ZnO samples were characterized by XRD, FTIR and SEM. The optical properties of the final products were investigated by UV-vis absorption spectrometer and photoluminescence. The formation mechanism was also discussed.

引用

页码：849 / 853

页数：5

共 50 条

[31] Microwave assisted synthesis of flower-like ZnO and effect of annealing atmosphere on its photoluminescence property [J].

Rai, Prabhakar ;

Kim, Seung-Gu ;

Yu, Yeon-Tae .

JOURNAL OF MATERIALS SCIENCE-MATERIALS IN ELECTRONICS, 2012, 23 (02) :344-348

[32] Optical properties and photocatalytic activities of spherical ZnO and flower-like ZnO structures synthesized by facile hydrothermal method [J].

Fang, Yongling ;

Li, Zhongyu ;

Xu, Song ;

Han, Dandan ;

Lu, Dayong .

JOURNAL OF ALLOYS AND COMPOUNDS, 2013, 575 :359-363

[33] Facile morphology-controlled hydrothermal synthesis of flower-like self-organized ZnO architectures [J].

Zhang, Rongxian ;

Yang, Xiaofei ;

Zhang, Du ;

Qin, Jieling ;

Lu, Chunyu ;

Ding, Heyi ;

Yan, Xuehua ;

Tang, Hua ;

Wang, Mingsong ;

Zhang, Qi .

CRYSTAL RESEARCH AND TECHNOLOGY, 2011, 46 (11) :1189-1194

[34] Microwave-assisted synthesis of flower-like β-FeSe microstructures [J].

Li, Mao-Lin ;

Yao, Qi-Zhi ;

Zhou, Gen-Tao ;

Fu, Sheng-Quan .

CRYSTENGCOMM, 2010, 12 (10) :3138-3144

[35] Hydrothermal synthesis of anatase flower-like nanostructures for photocatalytic degradation of dye [J].

Zhang, Li ;

Ding, Qianqian ;

Zhou, Ying .

CRYSTAL RESEARCH AND TECHNOLOGY, 2011, 46 (11) :1202-1206

[36] Hydrothermal Synthesis and Luminescence Properties of CePO4:Tb Flower-Like Clusters [J].

Bao Jin-rong ;

Zhu Xiao-wei ;

Jin Shu-xin ;

Lu Yue ;

Xiong Li-chao ;

Li Chang-fu ;

Li Wen-xian .

SPECTROSCOPY AND SPECTRAL ANALYSIS, 2013, 33 (01) :27-30

[37] Long chain polymer assisted synthesis of flower-like cadmium sulfide nanorods via hydrothermal process [J].

Salavati-Niasari, Masoud ;

Davar, Fatemeh ;

Loghman-Estarki, Mohammad Reza .

JOURNAL OF ALLOYS AND COMPOUNDS, 2009, 481 (1-2) :776-780

[38] A new method for synthesis of ZnO flower-like nanostructures and their photocatalytic performance [J].

Zou, Xinwei ;

Ke, Jun ;

Hao, Jianying ;

Yan, Xiaoyan ;

Tian, Yuming .

PHYSICA B-CONDENSED MATTER, 2022, 624

[39] A novel synthesis and excellent photodegradation of flower-like ZnO hierarchical microspheres [J].

Zhan, Jinxin ;

Dong, Hongxing ;

Liu, Yang ;

Wang, Yinglei ;

Chen, Zhanghai ;

Zhang, Long .

CRYSTENGCOMM, 2013, 15 (47) :10272-10277

[40] Multibranched flower-like ZnO particles from eco-friendly hydrothermal synthesis as green antimicrobials in agriculture [J].

Chang, Tao-Ho ;

Lu, Ying-Chun ;

Yang, Min-Jung ;

Huang, Jenn-Wen ;

Chang, Pi-Fang Linda ;

Hsueh, Han-Yu .

JOURNAL OF CLEANER PRODUCTION, 2020, 262

← 1 2 3 4 5 →