Application of high-performance liquid chromatography to the determination of the concentration of lichen secondary metabolites

被引：2

作者：

Prokopiev, I. A. ^{[1
]}

Shavarda, A. L. ^{[2
,3
]}

Filippova, G. V. ^{[1
]}

Shein, A. A. ^{[1
]}

机构：

[1] Russian Acad Sci, Siberian Branch, Inst Biol Problems Cryolithozone, Yakutsk 677980, Russia

[2] Russian Acad Sci, Komarov Bot Inst, St Petersburg 197376, Russia

[3] St Petersburg State Univ, Resource Ctr Dev Mol & Cellular Technol, Sci Pk, St Petersburg 194034, Russia

来源：

JOURNAL OF ANALYTICAL CHEMISTRY | 2017年 / 72卷 / 11期

基金：

俄罗斯基础研究基金会;

关键词：

lichen substances; preparative flash chromatography; HPLC; mass spectrometry; Cladonia genus; Yakutia; IDENTIFICATION; SUBSTANCES; CLADONIA;

D O I：

10.1134/S1061934817090088

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

Preparative isolation of aromatic metabolites from lichens of the Cladonia genus (C. stellaris, C. arbuscula, C. amaurocraea, and C. rangiferina) growing in Central Yakutia was carried out. Identification by IR, UV, and time-of-flight mass spectrometry has shown that the isolated compounds belong to the group of lichen substances. It was shown that the component composition of the studied lichens corresponds to the previously described one. At the same time, the concentration of perlatolic and barbatic acids in C. stellaris and C. amaurocrae lichens, respectively, growing in Central Yakutia found by HPLC is higher than in similar types of temperate climatic zones.

引用

页码：1178 / 1183

页数：6

共 14 条

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