Template synthesis and characterization of molybdenum disulfide nanotubules

被引:22
作者
Yu, Dongbo [1 ]
Feng, Yi [1 ]
Zhu, Yanfang [1 ]
Zhang, Xuebin [1 ]
Li, Bin [1 ]
Liu, Huiqiang [1 ]
机构
[1] Hefei Univ Technology, Sch Mat Sci & Engn, Hefei 230009, Anhui, Peoples R China
基金
中国国家自然科学基金;
关键词
Nanostructure; Microstructure; MOS2; NANOTUBES; CONTROLLED FABRICATION; CARBON NANOTUBES; POROUS ALUMINA; NANOWIRES; LITHIUM; NANOPARTICLES; TUBES;
D O I
10.1016/j.materresbull.2011.04.018
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Molybdenum disulfide nanotubules were prepared by thermal decomposition of ammonium thiomolybdate ((NH(4))(2)MoS(4)) precursors on anodized aluminum oxide template. Large quantities of hollow MoS(2) nanotubules with the bamboo-like structure were obtained. The morphology and structures of MoS(2) tubules were characterized by scanning electron microscopy, high-resolution transmission electron microscopy, energy dispersive spectroscopy, electron diffraction and optical absorption spectroscopy. MoS(2) nanotubules completely reflected the three-dimensional structure of nanopores in template. The properties of Mo-S chemical bonds in lattice structure and the wetting state between porous surface and precursor have a great effect on the formation of sections in nanotubules, the ridges in the nanopores also play a very special role of this formation. (c) 2011 Elsevier Ltd. All rights reserved.
引用
收藏
页码:1504 / 1509
页数:6
相关论文
共 26 条
[1]   Synthesis of MoS2 nanorods and their catalytic test in the HDS of dibenzothiophene [J].
Albiter, M. A. ;
Huirache-Acuna, R. ;
Paraguay-Delgado, F. ;
Rico, J. L. ;
Alonso-Nunez, G. .
NANOTECHNOLOGY, 2006, 17 (14) :3473-3481
[2]   Synthesis of open-ended MoS2 nanotubes and the application as the catalyst of methanation [J].
Chen, J ;
Li, SL ;
Xu, Q ;
Tanaka, K .
CHEMICAL COMMUNICATIONS, 2002, (16) :1722-1723
[3]   Thin films of fullerene-like MoS2 nanoparticles with ultra-low friction and wear [J].
Chhowalla, M ;
Amaratunga, GAJ .
NATURE, 2000, 407 (6801) :164-167
[4]   Bulk synthesis of inorganic fullerene-like MS(2) (M=Mo, W) from the respective trioxides and the reaction mechanism [J].
Feldman, Y ;
Frey, GL ;
Homyonfer, M ;
Lyakhovitskaya, V ;
Margulis, L ;
Cohen, H ;
Hodes, G ;
Hutchison, JL ;
Tenne, R .
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1996, 118 (23) :5362-5367
[5]   Synthesis of molybdenum disulfide (MoS2) for lithium ion battery applications [J].
Feng, Chuanqi ;
Ma, Jun ;
Li, Hua ;
Zeng, Rong ;
Guo, Zaiping ;
Liu, Huakun .
MATERIALS RESEARCH BULLETIN, 2009, 44 (09) :1811-1815
[6]   Magnetic properties of MoS2 nanotubes doped with lithium [J].
Jaglicic, Z ;
Jeromen, A ;
Trontelj, Z ;
Mihailovic, D ;
Arcon, D ;
Remskar, M ;
Mrzel, A ;
Dominko, R ;
Gaberscek, M ;
Martinez-Agudo, JM ;
Gómez-Garcia, CJ ;
Coronado, E .
POLYHEDRON, 2003, 22 (14-17) :2293-2295
[7]   Preparation of ultrafine carbon tubes in nanochannels of an anodic aluminum oxide film [J].
Kyotani, T ;
Tsai, LF ;
Tomita, A .
CHEMISTRY OF MATERIALS, 1996, 8 (08) :2109-2113
[8]   Investigation of micro-tribological behavior of MS2 nanotubes [J].
Li, Changsheng ;
Yan, Kehong ;
Li, Junmao ;
Shen, Xiaoping ;
Chen, Kangmin .
NANOSCIENCE AND TECHNOLOGY, PTS 1 AND 2, 2007, 121-123 :785-788
[9]   Templated deposition of MoS2 nanotubules using single source precursor and studies of their optical limiting properties [J].
Loh, KP ;
Zhang, H ;
Chen, WZ ;
Ji, W .
JOURNAL OF PHYSICAL CHEMISTRY B, 2006, 110 (03) :1235-1239
[10]   Controlled fabrication of hierarchically branched nanopores, nanotubes, and nanowires [J].
Meng, GW ;
Jung, YJ ;
Cao, AY ;
Vajtai, R ;
Ajayan, PM .
PROCEEDINGS OF THE NATIONAL ACADEMY OF SCIENCES OF THE UNITED STATES OF AMERICA, 2005, 102 (20) :7074-7078