Synthesis of new surface-active substances

被引:1
作者
Markowski, Jaroslaw [1 ]
Krasodomski, Wojciech [1 ]
机构
[1] Inst Nafty & Gazu Panstwowy Inst Badawczy, Zakladzie Dodatkow & Nowych Technol Chem, Krakow, Poland
来源
PRZEMYSL CHEMICZNY | 2016年 / 95卷 / 05期
关键词
D O I
10.15199/62.2016.5.4
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
Ten Mannich bases were synthesized in reaction of CH2O or lauryl aldehyde with Me2N(CH)(3)NH2 and p-RC6H4OH (R = Me, OMe, NO2, C12H5) or PhOMe at 45 degrees C optionally under microwave irradn. under lab. conditions. The bases were added to a base diesel oil studied then for homogeneity and interphase tension. Use of microwave heating resulted in a substantial acceleration of the Mannich reaction.
引用
收藏
页码:920 / 927
页数:8
相关论文
共 13 条
[1]  
[Anonymous], 2001, Patent No. [WO/2001/042399, 2001042399]
[2]  
[Anonymous], 2013, Pat, Patent No. [8557003B2, 8557003]
[3]   Microwave enhanced synthesis [J].
Caddick, Stephen ;
Fitzmaurice, Richard .
TETRAHEDRON, 2009, 65 (17) :3325-3355
[4]  
Folkson R, 2014, WOODHEAD PUBL SER EN, P1
[5]   Novel process windows - Concept, proposition and evaluation methodology, and intensified superheated processing [J].
Hessel, Volker ;
Cortese, B. ;
de Croon, M. H. J. M. .
CHEMICAL ENGINEERING SCIENCE, 2011, 66 (07) :1426-1448
[6]  
Ionescu M., 2005, Rapra Technology
[7]   A microwave-enhanced, solventless Mannich condensation of terminal alkynes and secondary amines with para-formaldehyde on cuprous iodide doped alumina [J].
Kabalka, GW ;
Zhou, LL ;
Wang, L ;
Pagni, RM .
TETRAHEDRON, 2006, 62 (05) :857-867
[8]  
Malfer D. J., 2004, US Patent, Patent No. [6,800,103, 6800103]
[9]  
Markowski J., 2014, NAFTA GAZ, P27
[10]  
Rehman W., 2010, BIOL POTENT MANNICH