MELAMINE-TRISULFONIC-ACID-CATALYZED TRIMETHYLSILYLATION OF ALCOHOLS AND PHENOLS

被引：3

作者：

Wu, Liqiang ^{[1
]}

Sun, Pengli ^{[1
]}

Yan, Fulin ^{[1
]}

机构：

[1] Xinxiang Med Univ, Sch Pharm, Xinxiang 453003, Henan, Peoples R China

来源：

PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS | 2011年 / 186卷 / 10期

关键词：

trimethylsilylation; hexamethyldisilazane; melamine trisulfonic acid; solvent-free; SOLVENT-FREE CONDITIONS; O-SILYLATION REACTIONS; HYDROXYL-GROUPS; REUSABLE CATALYST; HIGHLY EFFICIENT; 1,1,1,3,3,3-HEXAMETHYLDISILAZANE HMDS; HEXAMETHYLDISILAZANE HMDS; HETEROGENEOUS CATALYST; PROTECTION; MILD;

D O I：

10.1080/10426507.2010.544272

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

A highly convenient method for the trimethylsilylation of alcohols and phenols via treatment by hexamethyldisilazane in the presence of elamine trisulfonic acid as a catalyst has been developed. A wide variety of hydroxyl groups were selectively protected under solvent-free conditions.

引用

页码：2055 / 2060

页数：6

共 29 条

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