NMR and X-ray diffraction study of the crystalline structure of polyacrylonitrile

被引：0
作者：
Berestova, SS
Shchirets, VS
Selikhova, VI
Polyakov, DK
Polyakova, GR
Zubov, YA
Polikarpov, VV
机构：
来源：
VYSOKOMOLEKULYARNYE SOEDINENIYA SERIYA A & SERIYA B | 1996年 / 38卷 / 09期
关键词：
D O I：
暂无
中图分类号：
O63 [高分子化学（高聚物）];
学科分类号：
070305 ; 080501 ; 081704 ;
摘要：
An attempt was made to establish the correlation between the tacticity of the molecular chain of polyacrylonitrile (PAN) obtained with different types of initiating systems and the crystallite dimensions. X-ray and NMR spectroscopic studies showed that the lateral dimensions of the crystallites are controlled mainly by the temperature of polymerization (and crystallization, respectively), whereas the longitudional dimensions along the molecular chain, by the polymer microtacticity.
引用
收藏
页码：1612 / 1613
页数：2
相关论文
共 50 条
[31]   X-ray diffraction study of the structure of detonation nanodiamonds [J].
A. N. Ozerin ;
T. S. Kurkin ;
L. A. Ozerina ;
V. Yu. Dolmatov .
Crystallography Reports, 2008, 53 :60-67
[32]   X-ray diffraction study of the structure of detonation nanodiamonds [J].
Ozerin, A. N. ;
Kurkin, T. S. ;
Ozerina, L. A. ;
Dolmatov, V. Yu. .
CRYSTALLOGRAPHY REPORTS, 2008, 53 (01) :60-67
[33]   Crystal structure of kappa-alumina: An X-ray powder diffraction, TEM and NMR study [J].
Ollivier, B ;
Retoux, R ;
Lacorre, P ;
Massiot, D ;
Ferey, G .
JOURNAL OF MATERIALS CHEMISTRY, 1997, 7 (06) :1049-1056
[34]   An X-Ray Diffraction Study on Crystalline and Mesomorphic Structures of Poly(diethylsiloxane) [J].
Katsuhiro Inomata ;
Kazami Yamamoto ;
Takuhei Nose .
Polymer Journal, 2000, 32 :1044-1048
[35]   X-RAY DIFFRACTION STUDY OF ACOUSTIC MODE PATTERNS IN CRYSTALLINE QUARTZ [J].
SPENCER, WJ .
APPLIED PHYSICS LETTERS, 1963, 2 (07) :133-135
[36]   X-Ray Diffraction Study on Crystalline and Osmotic Swelling of a Layered Titanate [J].
Sasaki, Takayoshi ;
Watanabe, Mamoru .
MOLECULAR CRYSTALS AND LIQUID CRYSTALS SCIENCE AND TECHNOLOGY SECTION A-MOLECULAR CRYSTALS AND LIQUID CRYSTALS, 1998, 311 :417-422
[37]   An in situ X-ray diffraction study of the reaction of Li with crystalline Si [J].
Li, Jing ;
Dahn, J. R. .
JOURNAL OF THE ELECTROCHEMICAL SOCIETY, 2007, 154 (03) :A156-A161
[38]   X-ray diffraction study on crystalline and osmotic swelling of a layered titanate [J].
Sasaki, Takayoshi ;
Watanabe, Mamoru .
Molecular Crystals and Liquid Crystals Science and Technology Section A: Molecular Crystals and Liquid Crystals, 1998, 311 :417-422
[39]   An X-ray diffraction study on crystalline and mesomorphic structures of poly(diethylsiloxane) [J].
Inomata, K ;
Yamamoto, K ;
Nose, T .
POLYMER JOURNAL, 2000, 32 (12) :1044-1048
[40]   NMR AND X-RAY STUDIES ON THE MORPHOLOGY OF THERMOREVERSIBLE POLYACRYLONITRILE GELS [J].
HERBERT, IR ;
TIPPING, A ;
BASHIR, Z .
JOURNAL OF POLYMER SCIENCE PART B-POLYMER PHYSICS, 1993, 31 (11) :1459-1470
12345