Preparation of the Sm3+ Doped ZnO-Al2O3-SiO2 Glass-Ceramics

被引:0
作者
Zhang, Hong-bo [1 ]
Wu, Ping [1 ]
Su, Chun-hui [1 ]
Zou, Xiang-yu [1 ]
Wang, Yi-min [1 ]
机构
[1] Changchun Univ Sci & Technol, Coll Chem & Environm Engn, Changchun 130022, Peoples R China
来源
PROCEEDINGS OF THE 7TH NATIONAL CONFERENCE ON CHINESE FUNCTIONAL MATERIALS AND APPLICATIONS (2010), VOLS 1-3 | 2010年
关键词
ZAS; glass-ceramics; Sm3+;
D O I
暂无
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
The Sm3+ doped ZnO-Al2O3-SiO2 system glass-ceramics were prepared by melting and crystallization. Its heat treatment system in different conditions were studied. The micro-structure and optical properties were studied by differential scanning calorimetry (DSC), X-ray diffraction (XRD), scanning electron microscopy (SEM), UV - visible - near infrared spectrophotometer (UV-Vis-NIR), fluorescence spectroscopy. The results show that the optimized heat treating system of Sm3+ doped ZnO-Al2O3-SiO2 system(ZAS) glass is 730 degrees C x lh, the main crystal phase is Zn2SiO4, and the second phase is ZnAl2O4. The grain diameter observed by SEM is 10-15 nm, the optical transmittance reaches about 86% in near-infrared region.
引用
收藏
页码:1682 / 1685
页数:4
相关论文
共 11 条
[1]  
Cheng Jin-shu, 2009, Journal of Wuhan University of Technology, V31, P95
[2]  
Cheng Jinshu, 2008, Journal of the Chinese Ceramic Society, V36, P1013
[3]  
Duan XL, 2003, MATER RES BULL, V38, P705, DOI 10.1016/S0025-5408(02)00009-6
[4]  
[侯朝霞 HOU Zhaoxia], 2007, [兵工学报, Acta Armamentarii], V28, P253
[5]  
Meng CX, 2005, CHINESE J INORG CHEM, V21, P464
[6]   Structural and optical properties of ZnO-Al2O3-SiO2 system glass-ceramics containing Ni2+-doped nanocrystals [J].
Suzuki, T ;
Horibuchi, K ;
Ohishi, Y .
JOURNAL OF NON-CRYSTALLINE SOLIDS, 2005, 351 (27-29) :2304-2309
[7]  
[田培静 TIAN Pei-jing], 2009, [武汉理工大学学报, Journal of Wuhan University of Technology], V31, P36
[8]  
WANG HY, 2004, J FUNCTIONAL MAT, V21, P98
[9]  
WU BT, 2007, J WUHAN UNIV TECHNOL, V29, P251
[10]  
Xue M, 2007, CHINESE J INORG CHEM, V23, P708