A new synthetic procedure for ordered mesoporous γ-alumina with a large surface area

被引:42
作者
Huang, Fei [1 ]
Zheng, Ying [1 ,2 ]
Cai, Guohui [2 ]
Zheng, Yong [2 ]
Xiao, Yihong [2 ]
Wei, Kemei [2 ]
机构
[1] Fujian Normal Univ, Coll Chem & Mat Sci, Fuzhou 350007, Fujian, Peoples R China
[2] Fuzhou Univ, Natl Engn Res Ctr Chem Fertilizer Catalyst, Fuzhou 350002, Fujian, Peoples R China
关键词
High surface area; Mesoporous; Alumina; p6mm hexagonal symmetry; CRYSTALLINE ALUMINA; FACILE SYNTHESIS; GAMMA-AL2O3;
D O I
10.1016/j.scriptamat.2010.04.037
中图分类号
TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
Ordered mesoporous alumina with a large surface area was successfully synthesized in this work. Employing P123 as a structure-directing agent, the ordered mesostructure was fabricated only when the molar ratio of salicylic acid to citric acid was 2, and the large surface area was attributed to the addition of salicylic acid. The resulting alumina possesses a surface area of 520.65 m(2) g(-1) and a pore volume of 0.82 cm(3) g(-1). The surface area is still 300.20 m(2) g(-1) even after being calcinated at 800 degrees C. Crown Copyright (C) 2010 Published by Elsevier Ltd. on behalf of Acta Materialia Inc. All rights reserved.
引用
收藏
页码:339 / 342
页数:4
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