Synthesis and X-ray crystal structure of bis-3,3′-(nitro-NNO-azoxy)-difurazanyl ether

被引：0

作者：

Sheremetev, AB ^{[1
]}

Semenov, SE ^{[1
]}

Kuzmin, VS ^{[1
]}

Strelenko, YA ^{[1
]}

Ioffe, SL ^{[1
]}

机构：

[1] Russian Acad Sci, ND Zelinskii Organ Chem Inst, Moscow 117913, Russia

来源：

CHEMISTRY-A EUROPEAN JOURNAL | 1998年 / 4卷 / 06期

关键词：

azo compounds; furazans; heterocycles; nitro groups; structure elucidation;

D O I：

10.1002/(SICI)1521-3765(19980615)4:6<1023::AID-CHEM1023>3.3.CO;2-I

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

Two approaches to the synthesis of bis-3,3'-(nitro-NNO-azoxy)difurazanyl ether 2 have been tested, that is, varying the sequence of the introduction of the nitro-NNO-azoxy group and ether bridge. Difurazanyl ether formation through base-promoted transformation of nitrofurazans has been studied in which the nitro groups were activated by ortho electron-withdrawing substituents such as nitro-NNO-azoxy and tert-butyl-NNO-azoxy groups. The nitro-NNO-azoxy group was formed by destructive N-nitration of the tert-butyl-NNO-azoxy group. The X-ray crystal structure of 2 is reported.

引用

页码：1023 / 1026

页数：4

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