A Rapid Combustion and Calcination Process for the Preparation of Magnetic ZnFe2O4 Nanoparticles

被引：14

作者：

Liu, Ruijiang ^{[1
,2
]}

Han, Jing ^{[1
]}

Fu, Hongxia ^{[1
]}

Lu, Yimin ^{[2
]}

Wang, Yanyan ^{[3
]}

机构：

[1] Jiangsu Univ, Sch Pharm, Zhenjiang 212013, Peoples R China

[2] Jiangsu Univ, Affiliated Kunshan Hosp, Kunshan 215300, Peoples R China

[3] Jiangsu Union Tech Inst, Lianyungang Tradit Chinese Med Branch, Lianyungang 222006, Peoples R China

来源：

NANOSCIENCE AND NANOTECHNOLOGY LETTERS | 2016年 / 8卷 / 03期

关键词：

ZnFe2O4; Nanoparticles; Rapid Combustion; Solvent Volume; Calcination Temperature; NANOARCHITECTONICS; NI;

D O I：

10.1166/nnl.2016.2104

中图分类号：

TB3 [工程材料学];

学科分类号：

0805 ; 080502 ;

摘要：

A rapid combustion and calcination process for the preparation of magnetic ZnFe2O4 nanoparticles was introduced. The experimental results showed that the single ferrite phase of ZnFe2O4 could be formed at 400 degrees C, and the volume of the solvent and the calcination temperature were two key factors to the properties of magnetic ZnFe2O4 nanoparticles: with the volume of absolute alcohol increasing from 10 mL to 30 mL, the average grain size of ZnFe2O4 nanoparticles calcined at 400 degrees C for 2 h with the heating rate of 3 degrees C/min increased from 8.6 nm to 17.9 nm, while the saturation magnetization increased from 0.3 Am-2/kg to 3.1 Am-2/kg, and with the calcination temperature increasing from 400 degrees C to 800 degrees C, the average grain size of ZnFe2O4 nanoparticles calcined for 2 h with absolute alcohol of 30 mL and the heating rate of 3 degrees C/min increased from 17.9 nm to 45.8 nm, the saturation magnetizations increased from 3.1 Am-2/kg to 8.9 Am-2/kg.

引用

页码：232 / 235

页数：4

共 15 条

[1] Functionalized Gold Nanoparticles: Synthesis, Properties and Applications-A Review [J].

Alex, Saji ;

Tiwari, Ashutosh .

JOURNAL OF NANOSCIENCE AND NANOTECHNOLOGY, 2015, 15 (03) :1869-1894

[2] Semiconductor-to-metallic flipping in a ZnFe2O4-graphene based smart nano-system: Temperature/microwave magneto-dielectric spectroscopy [J].

Ameer, Shahid ;

Gul, Iftikhar Hussain ;

Mahmood, Nasir ;

Mujahid, Muhammad .

MATERIALS CHARACTERIZATION, 2015, 99 :254-265

[3] Nanoarchitectonics for Dynamic Functional Materials from Atomic-/Molecular-Level Manipulation to Macroscopic Action [J].

Ariga, Katsuhiko ;

Li, Junbai ;

Fei, Jinbo ;

Ji, Qingmin ;

Hill, Jonathan P. .

ADVANCED MATERIALS, 2016, 28 (06) :1251-1286

[4]

Costa A.C.F.M., 2012, J MATER SCI, V37, P3569

[5] Facile reduction of nitrophenols: Comparative catalytic efficiency of MFe2O4 (M = Ni, Cu, Zn) nano ferrites [J].

Goyal, Ankita ;

Bansal, S. ;

Singhal, Sonal .

INTERNATIONAL JOURNAL OF HYDROGEN ENERGY, 2014, 39 (10) :4895-4908

[6] Synthesis and characterization of ZnFe2O4 nanoparticles and its biomedical applications [J].

Hoque, S. Manjura ;

Hossain, Md. Sazzad ;

Choudhury, Shamima ;

Akhter, S. ;

Hyder, F. .

MATERIALS LETTERS, 2016, 162 :60-63

[7] Chemical synthesis and magnetic investigations on Cr3+ substituted Zn-ferrite superparamagnetic nano-particles [J].

Kumari, Naveen ;

Kumar, Vinod ;

Khasa, S. ;

Singh, S. K. .

CERAMICS INTERNATIONAL, 2015, 41 (01) :1907-1911

[8] Functional Nanoparticles in Targeting Glioma Diagnosis and Therapies [J].

Li, Minghui ;

Deng, Hongbing ;

Peng, Haisheng ;

Wang, Qun .

JOURNAL OF NANOSCIENCE AND NANOTECHNOLOGY, 2014, 14 (01) :415-432

[9] A facile sol combustion and calcination process for the preparation of magnetic Ni0.5Zn0.5Fe2O4 nanopowders and their adsorption behaviors of Congo red [J].

Liu, Ruijiang ;

Fu, Hongxia ;

Yin, Hengbo ;

Wang, Peng ;

Lu, Lu ;

Tao, Yuting .

POWDER TECHNOLOGY, 2015, 274 :418-425

[10] Mossbauer and magnetic studies of nanocrystalline zinc ferrites synthesized by microwave combustion method [J].

Mahmoud, Mohamed ;

Hassan, Azza Mohamed ;

Ahmed, Mamdouh Abdel Aal ;

Zhu, Kaixin ;

Ganeshraja, Ayyakannu Sundaram ;

Wang, Junhu .

HYPERFINE INTERACTIONS, 2016, 237 :1-11

← 1 2 →