Efficient and convenient one-pot synthesis of phosphoramidates and phosphates

被引：19
|
作者：
Gupta, A. K. [1 ]
Acharya, J. [1 ]
Dubey, D. K. [1 ]
Kaushik, M. P. [1 ]
机构：
[1] Def Res & Dev Estab, Proc Technol Dev Div, Gwalior 474002, MP, India
来源：
SYNTHETIC COMMUNICATIONS | 2007年 / 37卷 / 19-21期
关键词：
dialkylphosphites; phosphates; phosphoramidates; trichloroisocyanuric acid;
D O I：
10.1080/00397910701483662
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
A simple and efficient one-pot method is described for the synthesis of phosphoramidates/phosphates in excellent yields from dialkylphosphites and trichloroisocyanuric acid in acetonitrile and subsequent treatment with dialkyl amines/ alcohols. The procedure is operationally simple, has reduced reaction times, and uses a one-pot procedure.
引用
收藏
页码：3403 / 3407
页数：5
相关论文
共 50 条
  • [21] A Convenient One-pot Synthesis of Chromenyl Acrylates and Acrylonitriles
    Lopes, Diogo
    Costa, Marta
    Loucano, Joao
    Proenca, Fernanda
    SYNLETT, 2020, 31 (13) : 1298 - 1302
  • [22] A convenient one-pot synthesis of cyclohexenic primary amines
    Barbot, F
    Aidene, M
    Miginiac, L
    SYNTHETIC COMMUNICATIONS, 1998, 28 (17) : 3279 - 3289
  • [23] Novel convenient one-pot method for the synthesis of indoloquinolines
    N. A. Aksenov
    A. Z. Gasanova
    G. M. Abakarov
    I. V. Aksenova
    A. V. Aksenov
    Russian Chemical Bulletin, 2019, 68 : 836 - 840
  • [24] CONVENIENT ONE-POT SYNTHESIS OF DL-PYROCIN
    SCOTT, F
    NKWELO, MM
    SYNTHETIC COMMUNICATIONS, 1985, 15 (12) : 1051 - 1056
  • [25] A convenient one-pot synthesis of 6-trifluoromethylpyridines
    Katsuyama, I
    Ogawa, S
    Nakamura, H
    Yamaguchi, Y
    Funabiki, K
    Matsui, M
    Muramatsu, H
    Shibata, K
    HETEROCYCLES, 1998, 48 (04) : 779 - 785
  • [26] A one-pot and convenient synthesis of coumarins in solventless system
    Shockravi, A
    Valizadeh, H
    Heravi, MM
    PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS, 2003, 178 (03) : 501 - 504
  • [27] A convenient one-pot synthesis of cyclohexenic primary amines
    Lab. de Synthèse Organique, URA 574 CNRS, Université de Poitiers, 40, avenue du Recteur Pineau, 86022 Poitiers, France
    Synth. Commun., 17 (3279-3289):
  • [28] Convenient one-pot synthesis and structures of pentaphenyltellurium monohalides
    Minoura, M
    Sagami, T
    Akiba, K
    ORGANOMETALLICS, 2001, 20 (12) : 2437 - 2439
  • [29] A CONVENIENT ONE-POT SYNTHESIS OF ALPHA-HALOACYLSILANES
    PAGE, PCB
    ROSENTHAL, S
    TETRAHEDRON LETTERS, 1986, 27 (44) : 5421 - 5422
  • [30] A CONVENIENT ONE-POT SYNTHESIS OF POLYENIC ENOL ETHERS
    VOQUANG, Y
    CARNIATO, D
    VOQUANG, L
    LEGOFFIC, F
    JOURNAL OF THE CHEMICAL SOCIETY-CHEMICAL COMMUNICATIONS, 1983, (24) : 1505 - 1506
12345