Diethyl 1,4-dioxo-6-(3-pyridyl)perhydro-2,3,4a,6,7a-pentaazacyclopenta[cd]indene-2a,7b-dicarboxylate1,2-dichoroethane solvate

被引:2
作者
Cao, Li-Ping [1 ]
Wang, Zhi-Guo
Hu, Yan
机构
[1] Cent China Normal Univ, Coll Chem, Key Lab Pest & Chem Biol Minist Educ, Wuhan 430079, Peoples R China
[2] Huangshi Inst Technol, Sch Chem & Mat Engn, Huangshi 435003, Peoples R China
来源
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2007年 / 63卷
关键词
D O I
10.1107/S1600536807054566
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
The main residue of the title compound, C18H22N6O6 center dot C2H4Cl2, is a derivative of glycoluril. The six-membered heterocycle adopts a chair conformation and shares two N atoms with two five-membered rings of the glycoluril unit to form the flexible sidewalls of a molecular clip. Two ethyl fragments and the solvent molecule are disordered; the site occupancy factors for the ethyl groups are 0.72/0.28 and 0.75/0.25 and for the solvent molecule 0.54/0.46. Intermolecular N-H center dot center dot center dot O and N-H center dot center dot center dot N hydrogen bonds link the cyclopenta[ cd] indene molecules into two-dimensional layers parallel to the bc plane.
引用
收藏
页码:O4540 / U3498
页数:12
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