Influence of aluminium-rich intermetallics on microstructure evolution and mechanical properties of friction stir alloyed Al-Fe alloy system

被引:22
作者
Sharma, Abhishek [1 ]
Morisada, Yoshiaki [1 ]
Fujii, Hidetoshi [1 ]
机构
[1] Osaka Univ, Joining & Welding Res Inst, Osaka 5670047, Japan
关键词
Aluminium (Al); Iron (Fe); Alloying; Friction stir processing (FSA); Intermetallic phases; Al13Fe4; IN-SITU; MATRIX COMPOSITES; NICKEL; FABRICATION; INTERFACE; BEHAVIOR; SILICON; IRON;
D O I
10.1016/j.jmapro.2021.05.073
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
In the present investigation, the Al-Fe alloy system is developed by using the solid-state friction stir alloying (FSA) technique. The objective is realized by using multiple passes (1-4) of FSA with 100% overlap at constant process parameters. The TEM analysis confirms the interfacial reaction between the Al and Fe particles leading to the formation of nano-sized hard and brittle Al13Fe4 intermetallic (IMC) phase. The SEM, EDS, and XRD analysis also indicates the existence of a very small amount of Al5Fe2 IMC layer at the Al-Fe interface. The microstructural analysis from EBSD confirms that the grain size is reduced from -27 mu m in the base material to -2 mu m in the 4 pass FSAed Al-Fe alloy through dynamic recrystallization mechanism. The microhardness in the SZ is increased by -14% in the 4 pass FSAed Al-Fe alloy as compared to that with 1 pass. The increased hardness of Al-Fe alloys as compared to the 4 passes processed Al alloy (without Fe) suggest that the Al-Fe alloys system presented here can be an alternative solution for underwater friction stir welding (UFSW) to compensate for the stir zone softening occurred by the high heat input process parameters or precipitate dissolution in the heat treatable Al alloys. The ultimate tensile strength and percentage elongation are increased by -30% and -48% in the 4 pass FSAed Al-Fe alloy as compared to the alloy fabricated at 1 pass, respectively. The increased strength and hardness of the 4 passes FSAed alloy is attributed to the increased reaction rate between Al and Fe particles owing to the higher heat input which results in the precipitation of a more number of Al13Fe4 IMC phases during 4 passes. Also, the uniform dispersion of nano-sized IMC phases in 4 passes FSAed alloy as compared to the alloy fabricated with 1 pass, contribute significantly to the dislocation blockade and dispersion strengthening mechanism. The shreds of evidence provided in the present investigation suggest that the precipitation hardening is the dominant strengthening mechanism in the Al-Fe alloy system as compared to the Hall-petch strengthening mechanism.
引用
收藏
页码:668 / 682
页数:15
相关论文
共 61 条
[1]   Surface alteration of aluminium alloy by an exfoliated graphitic tribolayer during friction surfacing using a consumable graphite rich tool [J].
Abhishek Sharma ;
Tripathi, Arpit ;
Narsimhachary, Damanapeta ;
Mahto, Raju Prasad ;
Paul, Jinu .
SURFACE TOPOGRAPHY-METROLOGY AND PROPERTIES, 2019, 7 (04)
[2]   In Situ Determination of Phase Transformations and Structural Changes During Non-Equilibrium Material Processing [J].
Alexandrov, Boian T. ;
Lippold, John C. .
IN-SITU STUDIES WITH PHOTONS, NEUTRONS AND ELECTRONS SCATTERING, 2010, :113-131
[3]   LASER ALLOYING OF ALUMINUM-ALLOYS WITH CHROMIUM [J].
ALMEIDA, A ;
ANJOS, M ;
VILAR, R ;
LI, R ;
FERREIRA, MGS ;
STEEN, WM ;
WATKINS, KG .
SURFACE & COATINGS TECHNOLOGY, 1995, 70 (2-3) :221-229
[4]   Surface melting of aluminum [J].
Alvarado, FDC ;
Rutkowski, JH ;
Urbaniak-Kucharczyk, A ;
Wojtczak, L .
THIN SOLID FILMS, 1998, 317 (1-2) :43-47
[5]   Influences on the formability and mechanical properties of 7000-aluminum alloys in hot and warm forming [J].
Behrens, B-A ;
Nuernberger, F. ;
Bonk, C. ;
Huebner, S. ;
Behrens, S. ;
Vogt, H. .
36TH IDDRG CONFERENCE - MATERIALS MODELLING AND TESTING FOR SHEET METAL FORMING, 2017, 896
[6]   Friction Stir Processing of Al with Mechanically Alloyed Al-TiO2-Graphite Powder: Microstructure and Mechanical Properties [J].
Beygi, R. ;
Mehrizi, M. Zarezadeh ;
Eisaabadi, G. B. .
JOURNAL OF MATERIALS ENGINEERING AND PERFORMANCE, 2017, 26 (03) :1455-1462
[7]   Microstructure and Impression Creep Behavior of Al Based Surface Composite Produced by Friction Stir Processing [J].
Bhat, Udaya K. ;
Udupa, Rajendra K. ;
Prakrathi, S. ;
Huilgol, Prashant .
TRANSACTIONS OF THE INDIAN INSTITUTE OF METALS, 2016, 69 (02) :623-627
[8]   Thermal stability of Al-Fe-Ni alloy at high temperatures [J].
Bian, Zeyu ;
Dai, Shihan ;
Wu, Liang ;
Chen, Zhe ;
Wang, Mingliang ;
Chen, Dong ;
Wang, Haowei .
JOURNAL OF MATERIALS RESEARCH AND TECHNOLOGY-JMR&T, 2019, 8 (03) :2538-2548
[9]   Kinetic interactions between solid iron and molten aluminium [J].
Bouayad, A ;
Gerometta, C ;
Belkebir, A ;
Ambari, A .
MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING, 2003, 363 (1-2) :53-61
[10]   Mechanical Properties of Nanometric Al2O3 Particulate-Reinforced Al-Al11Ce3 Composites Produced by Friction Stir Processing [J].
Chen, Chin-Fu ;
Kao, Po-We ;
Chang, Liuwen ;
Ho, New-Jin .
MATERIALS TRANSACTIONS, 2010, 51 (05) :933-938