1,4-bis(3-pyridylaminomethyl)benzene

被引:11
作者
Zhu, Li-Na [1 ]
Gao, Shan [1 ]
Huo, Li-Hua [1 ]
机构
[1] Heilongjiang Univ, Sch Chem & Mat Sci, Harbin 150080, Peoples R China
关键词
D O I
10.1107/S1600536807052476
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
A new flexible bis(pyridyl) complex, C18H18N4, was prepared by the reaction of terephthalaldehyde with 3-aminopyridine. The molecule is centrosymmetric. Mononuclear units are linked into a one- dimensional chain by intermolecular N- H center dot center dot center dot N hydrogen bonds. The dihedral angle bentween the pyridyl ring and the central benzene ring is 63.6 (2)degrees.
引用
收藏
页码:O4459 / U4750
页数:7
相关论文
共 8 条
[1]  
Higashi T., 1995, ABSCOR
[2]  
JOHNSON CK, 1976, ORNL5138 ORTEP2
[3]  
MUNNO GD, 1999, J CHEM SOC DA, P1813
[4]  
Park SH, 1998, B KOR CHEM SOC, V19, P79
[5]  
Rigaku, 1998, RAPID AUTO
[6]  
RIGAKU MSC, 2002, CRYSTALSTRUCTURE
[7]  
Sheldrick G., 2017, SHELX2017, Programs for Crystal Structure Determination
[8]   1,4-bis(pyridine-2-aminomethyl)benzene [J].
Zou, RY ;
Xu, FB ;
Li, QS ;
Song, HB ;
Lv, H ;
Zhang, ZZ .
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2003, 59 :O1312-O1313