4,4′-Bipyridine-1,1′-diium 2,3,5,6-tetrabromoterephthalate dihydrate

被引：5
作者：
Kumagai, Hitoshi [1 ]
Kawata, Satoshi [2 ]
机构：
[1] Inst Mol Sci, Aichi, Japan
[2] Fukuoka Univ, Dept Chem, Fukuoka 8140180, Japan
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2011年 / 67卷
基金：
日本学术振兴会;
关键词：
data-to-parameter ratio = 17.2; mean σ(C-C) = 0.005 Å; R factor = 0.031; single-crystal X-ray study; T = 293 K; wR factor = 0.086;
D O I：
10.1107/S1600536811035926
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
The title compound, C10H10N22+center dot C8Br4O42-center dot 2H(2)O, consists of a tetrabromoterephthalate dianion, a 4,4'-bipyridinium dication and two solvent water molecules. Crystallographic inversion centers are situated at the center of the aromatic ring of the dianion as well as at the midpoint of the carbon-carbon bond connecting the pyridine rings in the dication. In the crystal, intermolecular N-H center dot center dot center dot O hydrogen-bonding interactions between tetrabromoterephthalate dianions and protonated 4,4'-bipyridinium dications result in the formation of a chain-like structure. Further O-H center dot center dot center dot O hydrogen bonds between carboxylate O atoms and water molecules lead to the formation of a two-dimensional network in the crystal structure.
引用
收藏
页码：O2636 / +
页数：9
相关论文
共 50 条
[11]   (2E)-3-(4-Cyanophenyl)-1-(4,4 ''-difluoro-5 '-methoxy-1,1 ':3 ',1 ''-terphenyl-4 '-yl)-prop-2-en-1-one [J].
Fun, Hoong-Kun ;
Loh, Wan-Sin ;
Samshuddin, S. ;
Narayana, B. ;
Sarojini, B. K. .
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 :O1877-+
[12]   5-(4,4"-Difluoro-5′-hydroxy-1,1′:3′,1"-terphenyl-4′-yl)-3-(morpholin-4-yl-methyl)-1,3,4-oxadiazole-2(3H)-thione [J].
Fun, Hoong-Kun ;
Arshad, Suhana ;
Samshuddin, S. ;
Narayana, B. ;
Sarojini, B. K. .
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 :O3372-U192
[13]   (2E)-3-(3-Bromo-4-methoxyphenyl)-1-(4,4"-difluoro-5′-methoxy-1,1′:3′,1"-terphenyl-4′-yl)prop-2-en-1-one [J].
Fun, Hoong-Kun ;
Shahani, Tara ;
Samshuddin, S. ;
Narayana, B. ;
Sarojini, B. K. .
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 :O3514-U453
[14]   N-(4,4 '-Dibromo-[1,1 '-biphenyl]-2-yl)benzamide [J].
Novina, J. Josephine ;
Vasuki, G. ;
Baheti, Abhishek ;
Thomas, K. R. Justin .
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2013, 69 :O222-+
[15]   Diaquabis(4,4′-bipyridine-κN)bis(2,4,5-trifluoro-3-hydroxybenzoato-κO1)manganese(II) [J].
Min, Chun-Gang ;
Yang, Xi-Kun .
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 :M1826-U463
[16]   (2E)-1-(4,4 ''-Difluoro-5 '-methoxy-1,1 ': 3 ',1 ''-terphenyl-4 '-yl)-3-[4-( methyl-sulfanyl) phenyl] prop-2-en-1-one [J].
Kant, Rajni ;
Gupta, Vivek K. ;
Kapoor, Kamini ;
Samshuddin, S. ;
Narayana, B. .
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 :02378-+
[17]   5,12-Dimethylpyrazino[1,2-a:4,5-a ']-dibenzimidazole-5,12-diium dichloride dihydrate [J].
Han, Jie ;
Zhao, Ming-gao ;
Zhang, Jun ;
Ma, Lan ;
Fan, Guang .
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 :O3398-+
[18]   (E,E)-4,4'-dimethyl-2,2'-(1,1'-dibenzyl-azino)diphenol [J].
Chang, Jian-Guo ;
Li, Ji-Kun .
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2007, 63 :O4061-U3155
[19]   catena-Poly[[[aqua(5-carboxypyridine-3-carboxylato-κN)copper(I)]-μ-4,4′-bipyridine-κ2N:N′]monohydrate] [J].
Liu, Gang ;
Qin, Gao .
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2012, 68 :M120-U412
[20]   Aqua[2,2 '-(propane-1,3-diyl) bis(5-carboxy-1H-imidazole-4-carboxylato)kappa N-4(3),O-4 : N-3 ',O-4 '](pyridine-kappa N)-cobalt(II)-4,4 '-bipyridine (1/1) [J].
Liu, Wei ;
Li, Xia .
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 :M1109-+
12345