Non-destructive evaluation of ceramic porosity using terahertz time-domain spectroscopy

被引:12
作者
Hakobyan, Davit [1 ]
Hamdi, Maher [1 ]
Redon, Olivier [1 ]
Ballestero, Anthony [2 ]
Mayaudon, Alexis [2 ]
Boyer, Laurence [2 ]
Durand, Olivier [2 ]
Abraham, Emmanuel [3 ]
机构
[1] CEA Tech Nouvelle Aquitaine, Coeur Bersol Batiment B,28 Ave Gustave Eiffel, F-33600 Pessac, France
[2] Parc Ester Technopole, Ctr Technol Transfers Ceram, 7 Rue Soyouz, F-87068 Limoges, France
[3] Univ Bordeaux, CNRS, LOMA, UMR 5798, F-33400 Talence, France
关键词
Porosity evaluation; Aluminum oxideAl(2)O(3); Ceramics; Non-destructive evaluation; Dielectric properties; Terahertz time-domain spectroscopy; EFFECTIVE PERMITTIVITY; ELECTRIC-CONDUCTIVITY; LOSS TANGENT; CONSTANTS; MEDIA;
D O I
10.1016/j.jeurceramsoc.2021.10.026
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
Dielectric constants of Al2O3 (alumina) ceramic samples have been measured with non-destructive terahertz time-domain spectroscopy. Using an effective medium approximation, we demonstrated that the relative permittivity can be used to evaluate the porous alumina samples, with porosity fractions ranging from 0% to 20% per volume. This result makes it possible to control sample porosity, a key material parameter related to mechanical strength under compression load, hardness and wear resistance, or thermal stability. We also employed terahertz time-domain spectroscopy to differentiate alumina samples fabricated with different grain sizes, or reveal a small fraction of impurities, such as 5%O of ZrO2, embedded in non-porous alumina. These results demonstrated the potential of terahertz radiation for non-destructive characterization of low loss high dielectric constant ceramics.
引用
收藏
页码:525 / 533
页数:9
相关论文
共 31 条
[1]   Terahertz study on porosity and mass fraction of active pharmaceutical ingredient of pharmaceutical tablets [J].
Bawuah, Prince ;
Tan, Nicholas ;
Tweneboah, Samuel Nana A. ;
Ervasti, Tuomas ;
Zeitler, J. Axel ;
Ketolainen, Jarkko ;
Peiponen, Kai-Erik .
EUROPEAN JOURNAL OF PHARMACEUTICS AND BIOPHARMACEUTICS, 2016, 105 :122-133
[2]   Temperature dependence of the permittivity and loss tangent of high-permittivity materials at terahertz frequencies [J].
Berdel, K ;
Rivas, JG ;
Bolívar, PH ;
de Maagt, P ;
Kurz, H .
IEEE TRANSACTIONS ON MICROWAVE THEORY AND TECHNIQUES, 2005, 53 (04) :1266-1271
[3]   Measurement of the dielectric constant and loss tangent of high dielectric-constant materials at terahertz frequencies [J].
Bolivar, PH ;
Brucherseifer, M ;
Rivas, JG ;
Gonzalo, R ;
Ederra, I ;
Reynolds, AL ;
de Maagt, P .
IEEE TRANSACTIONS ON MICROWAVE THEORY AND TECHNIQUES, 2003, 51 (04) :1062-1066
[4]   Effective permittivity of porous media: a critical analysis of the complex refractive index model [J].
Brovelli, Alessandro ;
Cassiani, Giorgio .
GEOPHYSICAL PROSPECTING, 2008, 56 (05) :715-727
[6]   Imaging with terahertz radiation [J].
Chan, Wai Lam ;
Deibel, Jason ;
Mittleman, Daniel M. .
REPORTS ON PROGRESS IN PHYSICS, 2007, 70 (08) :1325-1379
[7]  
Choy T. C., 2016, Effective Medium Theory: Principles and Applications
[8]   A mathematical treatment of the electric conductivity and capacity of disperse systems I The electric conductivity of a suspension of homogenous spheroids [J].
Frickl, H .
PHYSICAL REVIEW, 1924, 24 (05) :575-587
[10]   Identification tag in the terahertz frequency domain using low-cost and tunable refractive index materials [J].
Hamdi, Maher ;
Garet, Frederic ;
Duvillaret, Lionel ;
Martinez, Philippe ;
Tourtollet, Guy Eymin Petot .
ANNALS OF TELECOMMUNICATIONS, 2013, 68 (7-8) :415-424