Synthesis and characterization of nanocrystalline niobium nitride powders

被引：21

作者：

Li, YG ^{[1
]}

Gao, L ^{[1
]}

机构：

[1] Chinese Acad Sci, Shanghai Inst Ceram, State Key Lab High Performance Ceram & Superfine, Shanghai 200050, Peoples R China

来源：

JOURNAL OF THE AMERICAN CERAMIC SOCIETY | 2003年 / 86卷 / 07期

关键词：

D O I：

10.1111/j.1151-2916.2003.tb03449.x

中图分类号：

TQ174 [陶瓷工业]; TB3 [工程材料学];

学科分类号：

0805 ; 080502 ;

摘要：

Nanocrystalline NbN powder was synthesized by the direct nitridation of amorphous Nb2O5 powder with high BET surface area. X-ray diffractometry analysis indicated that the cubic-phase NbN powder could be obtained by nitridation at 650degrees-800degreesC for 3-8 h. Transmission electron microscopy images showed that the particle sizes were in the range of 15-40 nm. The effect of the nitridation temperature and holding time on the powder properties was discussed.

引用

页码：1205 / 1207

页数：3

共 14 条

[1] EFFECT OF METAL-PARTICLE MORPHOLOGY ON THE COMBUSTION OF REFRACTORY-METALS IN NITROGEN
AGRAFIOTIS, CC
PUSZYNSKI, JA
HLAVACEK, V
[J]. JOURNAL OF THE AMERICAN CERAMIC SOCIETY, 1991, 74 (11) : 2912 - 2917
[2] Formation of niobium nitride by rapid thermal processing
Angelkort, C
Lewalter, H
Warbichler, P
Hofer, F
Bock, W
Kolbesen, BO
[J]. SPECTROCHIMICA ACTA PART A-MOLECULAR AND BIOMOLECULAR SPECTROSCOPY, 2001, 57 (10) : 2077 - 2089
[3] AMMONOLYSIS PRODUCTS OF THE DIALKYLAMIDES OF TITANIUM, ZIRCONIUM, AND NIOBIUM AS PRECURSORS TO METAL NITRIDES
BROWN, GM
MAYA, L
[J]. JOURNAL OF THE AMERICAN CERAMIC SOCIETY, 1988, 71 (01) : 78 - 82
[4] Effect of pressure on the composition and superconducting Tc value of NbN prepared by combustion synthesis
Buscaglia, V
Caracciolo, F
Ferretti, M
Minguzzi, M
Musenich, R
[J]. JOURNAL OF ALLOYS AND COMPOUNDS, 1998, 266 (1-2) : 201 - 206
[5] Synthesis of transition-metal nitrides from nanoscale metal particles prepared by homogeneous reduction of metal halides with an alkalide
Chen, XZ
Dye, JL
Eick, HA
Elder, SH
Tsai, KL
[J]. CHEMISTRY OF MATERIALS, 1997, 9 (05) : 1172 - 1176
[6] STUDY OF NIOBIUM NITRIDES FOR SUPERCONDUCTING RF CAVITIES
FABBRICATORE, P
FERNANDES, P
GUALCO, GC
MERLO, F
MUSENICH, R
PARODI, R
[J]. JOURNAL OF APPLIED PHYSICS, 1989, 66 (12) : 5944 - 5949
[7] Herle PS, 1997, J SOLID STATE CHEM, V134, P120
[8] PREPARATION OF HIGH-SURFACE-AREA TRANSITION-METAL NITRIDES - MO2N AND MON
JAGGERS, CH
MICHAELS, JN
STACY, AM
[J]. CHEMISTRY OF MATERIALS, 1990, 2 (02) : 150 - 157
[9] Synthesis of nanocrystalline titanium nitride powders by direct nitridation of titanium oxide
Li, JG
Gao, L
Sun, J
Zhang, QH
Guo, JK
Yan, DS
[J]. JOURNAL OF THE AMERICAN CERAMIC SOCIETY, 2001, 84 (12) : 3045 - 3047
[10] Li YG, 2002, J AM CERAM SOC, V85, P1294

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