Characterization of nanodimensional Ni-Zn ferrite prepared by mechanochemical and thermal methods

被引:9
作者
Manova, E. [1 ]
Paneva, D. [1 ]
Kunev, B. [1 ]
Riviere, E. [2 ]
Estournes, C. [3 ]
Mitov, I. [1 ]
机构
[1] Bulgarian Acad Sci, Inst Catalysis, Acad G Bonchev St,Block 11, BU-1113 Sofia, Bulgaria
[2] Inst Chimie Mol Mat Orsay, F-91405 Orsay, France
[3] CNRS, Inst Carnot, F-31062 Toulouse, France
来源
INTERNATIONAL CONFERENCE ON THE APPLICATIONS OF THE MOSSBAUER EFFECT (ICAME 2009) | 2010年 / 217卷
关键词
NANOPARTICLES;
D O I
10.1088/1742-6596/217/1/012102
中图分类号
O59 [应用物理学];
学科分类号
摘要
Nickel zinc ferrite nanoparticles, Ni1-xZnxFe2O4 (x = 0, 0.2, 0.5, 0.8, 1.0), with dimensions below 10 nm have been prepared by combining chemical precipitation with high-energy ball milling. For comparison, their analogues obtained by thermal synthesis have also been studied. Mossbauer spectroscopy, X-ray diffraction, and magnetic measurements are used for the characterization of the obtained materials. X-ray diffraction shows that after 3h of mechanical treatment ferrites containing zinc are formed, while 6h of treatment is needed to obtain NiFe2O4. The magnetic properties of the samples exhibit a strong dependence on the phase composition, particle size and preparation method.
引用
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页数:4
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