3-Ethyl-9-phenyl-2-tosyl-2,3,3a,4,9,9a-hexahydro-1H-pyrrolo[3,4-b]quinoline

被引：3

作者：

Sudha, D. ^{[1
]}

Chinnakali, K. ^{[1
]}

Jayagobi, M. ^{[2
]}

Raghunathan, R. ^{[2
]}

Fun, Hoong-Kun ^{[3
]}

机构：

[1] Anna Univ, Dept Phys, Madras 600025, Tamil Nadu, India

[2] Univ Madras, Dept Organ Chem, Madras 600025, Tamil Nadu, India

[3] Univ Sains Malaysia, Sch Phys, X Ray Crystallog Unit, George Town 11800, Malaysia

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2008年 / 64卷

关键词：

D O I：

10.1107/S1600536808000482

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

In the molecule of the title compound, C26H28N2O2S, the pyrrolidine ring adopts an envelope conformation and the tetrahydropyridine ring is in a half-chair conformation; these two rings are trans-fused. The dihedral angle between the pyridine- and sulfonyl-bound benzene rings is 36.15 (5)degrees. In the crystalline state, the molecules are linked into a two-dimensional network parallel to the ab plane by C-H center dot center dot center dot O and C-H center dot center dot center dot pi interactions.

引用

页码：O425 / U2176

页数：12

共 12 条

[1]

ANZINI M, 1990, FARMACO, V45, P1169

[2]

ANZINI M, 1992, FARMACO, V47, P191

[3]

*BRUK AXS INC, 2005, APEX2 VERS 1 27 SAIN

[4] GENERAL DEFINITION OF RING PUCKERING COORDINATES [J].

CREMER, D ;

POPLE, JA .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1975, 97 (06) :1354-1358

[5] INTERFERON INDUCING ACTIVITIES OF DERIVATIVES OF 1,3-DIMETHYL-4-(3-DIMETHYLAMINOPROPYLAMINO)-1H-PYRAZOLO[3,4-B]QUINOLINE AND RELATED COMPOUNDS [J].

CRENSHAW, RR ;

LUKE, GM ;

SIMINOFF, P .

JOURNAL OF MEDICINAL CHEMISTRY, 1976, 19 (02) :262-275

[6]

Duax WL, 1976, TOP STEREOCHEM, V9, P271

[7] Pyridone carboxylic acids as antibacterial agents. 18. Pyrroloquinolones and pyrazoloquinolones as potential antibacterial agents. Synthesis and antibacterial activity [J].

Fujita, M ;

Egawa, H ;

Miyamoto, T ;

Nakano, J ;

Matsumoto, J .

EUROPEAN JOURNAL OF MEDICINAL CHEMISTRY, 1996, 31 (12) :981-988

[8]

Sheldrick GM, 2015, ACTA CRYSTALLOGR C, V71, P3, DOI [10.1107/S2053229614024218, 10.1107/S0108767307043930]

[9] Single-crystal structure validation with the program PLATON [J].

Spek, AL .

JOURNAL OF APPLIED CRYSTALLOGRAPHY, 2003, 36 :7-13

[10] 7-bromo-3-ethyl-9-phenyl-2-tosyl-pyrrolo[3,4-b]quinoline [J].

Sudha, D. ;

Chinnakali, K. ;

Jayagobi, M. ;

Raghunathan, R. ;

Fun, Hoong-Kun .

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2008, 64 :0134-U3694

← 1 2 →