Ethyl 4-(3-bromo-2-thienyl)-2-oxo-6-phenylcyclohex-3-ene-1-carboxylate

被引：7

作者：

Fischer, Andreas ^{[1
]}

Yathirajan, H. S. ^{[2
]}

Ashalatha, B. V. ^{[3
]}

Narayana, B. ^{[3
]}

Sarojini, B. K. ^{[4
]}

机构：

[1] Royal Inst Technol KTH, Sch Chem Sci & Engn, S-10044 Stockholm, Sweden

[2] Univ Mysore, Dept Studies Chem, Mysore 570006, Karnataka, India

[3] Mangalore Univ, Dept Chem, Mangalagangothri 574199, Karnataka, India

[4] PA Coll Engn, Dept Chem, Mangalore 574153, India

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2008年 / 64卷

关键词：

D O I：

10.1107/S1600536808002717

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

The title compound, C19H17BrO3S, crystallizes with two molecules in the asymmetric unit. The methyl group of one molecule is disordered approximately equally over two positions. The dihedral angles between the thiophene and phenyl groups are 68.5 (2) and 67.5 (2)degrees in the two molecules.

引用

页码：O560 / U861

页数：12

共 12 条

[1]

BRANDENBURG K, 2007, DIAMOND RELEASE 3 1E

[2]

Dimmock JR, 1999, CURR MED CHEM, V6, P1125

[3] An intensity evaluation method:: EVAL-14 [J].

Duisenberg, AJM ;

Kroon-Batenburg, LMJ ;

Schreurs, AMM .

JOURNAL OF APPLIED CRYSTALLOGRAPHY, 2003, 36 :220-229

[4] INDEXING IN SINGLE-CRYSTAL DIFFRACTOMETRY WITH AN OBSTINATE LIST OF REFLECTIONS [J].

DUISENBERG, AJM .

JOURNAL OF APPLIED CRYSTALLOGRAPHY, 1992, 25 :92-96

[5] (7RS,8SR)-ethyl 6-(1,3-benzodioxol-5-yl)-3-(3-bromo-2-thienyl)-2-oxocyclohex-3-ene-1-carboxylate [J].

Fischer, Andreas ;

Yathirajan, H. S. ;

Ashalatha, B. V. ;

Narayana, B. ;

Sarojin, B. K. .

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2007, 63 :O3616-U4513

[6] (8RS,9SR)-Ethyl4-(3-bromothien-2-yl)-6(2-furyl)-2-oxocyclohex-3-ene-1-carboxylate [J].

Fischer, Andreas ;

Yathirajan, H. S. ;

Ashalatha, B. V. ;

Narayana, B. ;

Sarojini, B. K. .

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2007, 63 :O254-O255

[7]

Herrendorf W., 1997, HABITUS

[8]

HOUSE HO, 1972, MODERN SYNTHETIC REA, P595

[9]

*NON BV, 1999, COLLECT

[10] A short history of SHELX [J].

Sheldrick, George M. .

ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES, 2008, 64 :112-122

← 1 2 →