Synthesis and Crystal Structure of (5-Methyl-3-phenyl-1H-pyrazol-1-yl)-[5-(p-tolylamino)-2H-1,2,3-triazol-4-yl]methanone

被引:1
作者
Cao, Zi-Ping [1 ]
Dong, Hong-Ru [1 ]
Shen, Guo-Liang [1 ]
Dong, Heng-Shan [1 ]
机构
[1] Lanzhou Univ, Coll Chem & Chem Engn, Inst Organ Chem, State Key Lab Appl Organ Chem, Lanzhou 730000, Gansu, Peoples R China
关键词
Pyrazole; Crystal structure; Synthesis; 2H-1,2,3-Triazole; 1H-1,2,3-Triazole; REARRANGEMENTS; DERIVATIVES;
D O I
10.1007/s10870-010-9798-3
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
(5-Methyl-3-phenyl-1H-pyrazol-1-yl)-[5-(p-tolylamino)-2H-1,2,3-triazol-4-yl]methanone was synthesized and characterized by H-1 NMR, MS and IR spectra data. The structure of title compound was identified by X-ray diffraction. Compound, C20H18N6O, Mr = 358.40, crystallizes in the triclinic space group P-1 with unit cell parameters a = 10.303(6), b = 12.489(7), c = 15.305(9) angstrom, alpha = 108.489(12), beta = 101.920(11), gamma = 96.971(13)A degrees, V = 1790.0(17) angstrom(3), Z = 4, Dx = 1.330 mg/cm(3). The final R was 0.0520.
引用
收藏
页码:1078 / 1081
页数:4
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