Tetraaquabis[4-(4H-1,2,4-triazol-4-yl)benzoato-κN1]nickel(II) decahydrate

被引：0

作者：

Sun, Weixuan ^{[2
]}

Yu, Yaqin ^{[2
]}

Wang, Guanjun ^{[1
]}

Wu, Xiaohui

机构：

[1] Jilin Univ, Dept Hematol, Hosp 1, Changchun 130021, Peoples R China

[2] Jilin Univ, Sch Publ Hlth, Dept Prevent Med, Changchun 130021, Peoples R China

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2012年 / 68卷

关键词：

Data-to-parameter ratio = 12.9; Mean σ(C-C) = 0.005 Å; R factor = 0.049; Single-crystal X-ray study; T = 293 K; wR factor = 0.119;

D O I：

10.1107/S1600536811051063

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

In the title compound, [Ni(C9H6N3O2)(2)(H2O)(4)]center dot 10H(2)O, the Ni-II ion lies on a twofold rotation axis and displays a slightly distorted octahedral geometry defined by two N atoms from two monodentate 4-(1,2,4-triazol-4-yl) benzoate ligands and four water molecules, two of which also lie on the twofold rotation axis. In the crystal, the complex molecules and uncoordinated water molecules are linked via intermolecular O-H center dot center dot center dot N and O-H center dot center dot center dot O hydrogen bonds, forming a three-dimensional supramolecular network. pi-pi interactions between the benzene rings provide additional stability of the crystal packing [centroid-centroid distance = 3.792 (2) angstrom].

引用

页码：M10 / +

页数：10

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